(5,6)-Connected 3D Metal-Organic Framework Based on Terphenyl-3,2",5",3′-tetracarboxylate: Synthesis, Structures, and Properties

被引：2
|
作者：
Wang, Hua-Rui [1 ]
Liu, Shi-Jiang [2 ]
机构：
[1] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang 471022, Peoples R China
[2] Luoyang Normal Univ, Coll Phys & Elect Informat, Luoyang, Peoples R China
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2016年 / 46卷 / 09期
关键词：
tetracarboxylate; assemble; topology; metal-organic framework; PHOSPHONATES; CRYSTAL; DESIGN; LIGAND;
D O I：
10.1080/15533174.2015.1137008
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
One metal-organic framework [Mn(tptc)(0.5)(bpp)] (1) (H(4)tptc D terphenyl-3,2 '',5 '',3 '-tetracarboxylic acid, bpp D 1,3-bis(4-pyridyl) propane) has been synthesized by the reaction of a tetracarboxylate and auxiliary pyridine-based ligands with Mn(II) ion under hydrothermal conditions. This complex was further studied by elemental analysis, IR spectroscopy, and X-ray crystallography. In the structure of 1, the alternately assembled 2D helical bilayers and pyridine pillars gives rise to a rare (5,6)-connected 3D pillared helical-layer MOF. In addition, thermal gravimetric analysis of 1 was also investigated.
引用
收藏
页码：1422 / 1425
页数：4
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