Scalable synthesis of catalysts for the Mizoroki-Heck cross coupling reaction: palladium nanoparticles assembled in a polymeric nanosphere

被引：21

作者：

Zou, Jianli ^{[1
]}

Iyer, K. Swaminathan ^{[1
]}

Stewart, Scott G.

Raston, Colin L. ^{[1
]}

机构：

[1] Univ Western Australia, Ctr Strateg Nanofabricat, Sch Biomed Biomol & Chem Sci, Crawley, WA 6009, Australia

来源：

NEW JOURNAL OF CHEMISTRY | 2011年 / 35卷 / 04期

基金：

澳大利亚研究理事会;

关键词：

SUPPORTED PALLADIUM; TETRAALKYLAMMONIUM SALTS; HETEROGENEOUS CATALYSIS; ORGANIC-CHEMISTRY; PD NANOPARTICLES; SUZUKI; ARYLATION; LIGANDS; CARBON; SIZE;

D O I：

10.1039/c0nj00898b

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Palladium nano-spheres 160 nm in diameter, as an assembly of uniform 5 nm nanoparticles, are accessible using a facile one step method under continuous flow on a spinning disc with hydrogen gas as the reducing agent. The stable colloidal system is an effective catalyst for the Mizoroki-Heck reaction, as established for the reaction between several aryl halides and n-butyl acrylate, and can be readily recycled without a change in their catalytic activity.

引用

页码：854 / 860

页数：7

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