3-(1-Chlorovinyl)-2,4,6-trimethoxy-benzaldehyde

被引：4
|
作者：
Panda, AK
Parthasarathy, MR
Errington, W [1 ]
机构：
[1] Univ Warwick, Dept Chem, Coventry CV4 7AL, W Midlands, England
[2] Univ Delhi, Dept Chem, Delhi 110007, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY | 2001年 / 57卷
关键词：
D O I：
10.1107/S0108270100014700
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The title compound, C12H13ClO4, was prepared from the Vilsmeier-Haack reaction on phloroacetophenone. The chlorovinyl and one of the methoxy substituents are twisted through about 75 degrees with respect to the aromatic plane, whilst the other substituents are almost coplanar with the ring. Intermolecular hydrogen bonding involving C-H . . .O interactions generates one-dimensional chains in the direction of the a axis.
引用
收藏
页码：102 / 103
页数：2
相关论文
共 50 条
  • [31] STRUCTURE OF 2,4,6-TRIMETHOXY-1,3,5-TRIMETHYL-2,4,6-TRIOXOCYCLOTRIPHOSPHAZANE N3ME3P3O3(OME)3
    ANSELL, GB
    BULLEN, GJ
    CHEMICAL COMMUNICATIONS, 1965, (20) : 493 - &
  • [32] Synthesis of (+)-(1S,4R)-1-(1-chlorovinyl)-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one
    Vostrikov, NS
    Vasikov, VZ
    Spirikhin, LV
    Miftakhov, MS
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2004, 40 (09) : 1371 - 1372
  • [33] 3-(Hydroxydiphenylmethyl)-2-(methoxymethoxy)benzaldehyde
    Chen, WZ
    Zeng, QL
    Fang, H
    Gao, YX
    Zhao, YF
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O869 - O870
  • [34] Synthesis of (+)-(1S,4R)-1-(1-chlorovinyl)-7,7-dimethyl-bicyclo[2.2.1]heptan-2-one
    N. S. Vostrikov
    V. Z. Vasikov
    L. V. Spirikhin
    M. S. Miftakhov
    Russian Journal of Organic Chemistry, 2004, 40 : 1371 - 1372
  • [35] Vibration modes studies of 3,4,5-trimethoxy benzaldehyde, 4-hydroxy-3-methoxy benzaldehyde and 4-chloro benzaldehyde Schiff base of 2-amino pyridine-A quantum chemical study
    Arora, Kishor
    Kumar, D.
    Burman, Kiran
    Agnihotri, Sonal
    Singh, Bhoop
    ORIENTAL JOURNAL OF CHEMISTRY, 2010, 26 (04) : 1361 - 1368
  • [36] (E)-1-(2-thienyl)-3-(2,4,5-trimethoxy-phenyl)prop-2-en-1-one
    Fun, Hoong-Kun
    Jebas, Samuel Robinson
    Patil, P. S.
    Dharmaprakash, S. M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1510 - U2467
  • [37] A novel synthesis of 2,4,4-trisubstituted 2-cyclopentenones by consecutive reaction of 1-chlorovinyl p-tolyl sulfoxides with acetonitrile and its homologues
    Satoh, T
    Wakasugi, D
    TETRAHEDRON LETTERS, 2003, 44 (40) : 7517 - 7520
  • [38] (E)-1-(4-Bromophenyl)-3-(2,4,6-trimethoxyphenyl)prop-2-en-1-one
    Chantrapromma, Suchada
    Suwunwong, Thitipone
    Karalai, Chatchanok
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O893 - U3178
  • [39] (E)-1-(4-Methoxyphenyl)-3-(2,4,6-trimethoxyphenyl)prop-2-en-1-one
    Cai, Yuepiao
    Wang, Zhankun
    Li, Zhe
    Zhang, Meiling
    Wu, Jianzhang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1432 - U853
  • [40] NEMATIC SOLVENT EFFECTS IN THE ISOMERIZATION OF 2,4,6-TRIMETHOXY-S-TRIAZINE
    BACON, WE
    KUO, JL
    BROWN, GH
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 1979, 56 (01): : 13 - 17
12345