Synthesis of snowflake-like multi-layered ZnO with controllable pore sizes and its photocatalytic property

被引：11
|
作者：
Jing, Qiang [1 ]
Fu, Wuyou [1 ]
Li, Wancheng [2 ]
Yang, Haibin [1 ]
Li, Minghui [1 ]
Ma, Jinwen [1 ]
Zhou, Xiaoming [1 ]
Sun, Meiling [1 ]
Zhao, Hui [1 ]
Zhang, Yanyan [1 ]
Zhao, Wenyan [1 ]
Zhang, Lina [1 ]
Chen, Hui [1 ]
机构：
[1] Jilin Univ, State Key Lab Superhard Mat, Changchun 130012, Peoples R China
[2] Jilin Univ, State Key Lab Integrated Optoelect, Coll Elect Sci & Engn, Changchun 130012, Peoples R China
来源：
APPLIED SURFACE SCIENCE | 2012年 / 258卷 / 08期
关键词：
Microporous materials; Multilayers; Chemical synthesis; Heat treatment; Photocatalysis; Photoluminescence spectroscopy; CAPACITY HYDROGEN STORAGE; METAL-ORGANIC FRAMEWORKS; NANOWIRE ARRAYS; OPTICAL-PROPERTIES; POROUS MATERIALS; PHOTOLUMINESCENCE; NANOPARTICLES; TEMPERATURE; PERFORMANCE; MECHANISMS;
D O I：
10.1016/j.apsusc.2011.11.123
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Snowflake-like multi-layered ZnO with porous structure is synthesized through a facile hydrothermal process and followed by calcinating process. The pore size of the multilayered ZnO is controlled by just regulating the calcination temperature. X-diffraction (XRD) patterns reveal that the precursor obtained by hydrothermal method is zinc hydroxide carbonate (ZnHC)(1), after being calcinated, pure wurtzite ZnO is got. TEM and SEM demonstrate the existence of the porosity and the variation of the pore size (ranges from tens of nanometers to hundreds of nanometers). The photocatalytic property is investigated by Xenon Lamp and sunlight. (C) 2011 Elsevier B. V. All rights reserved.
引用
收藏
页码：3604 / 3610
页数：7
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