MCM-41-supported metal bis[(perfluoroalkyl)sulfonyl]imides as heterogeneous catalysts for aromatic nitration

被引：29

作者：

Yuan, YB ^{[1
]}

Nie, J ^{[1
]}

Zhang, ZB ^{[1
]}

Wang, SJ ^{[1
]}

机构：

[1] Huazhong Univ Sci & Technol, Dept Chem, Wuhan 430074, Peoples R China

来源：

APPLIED CATALYSIS A-GENERAL | 2005年 / 295卷 / 02期

关键词：

MCM-41; metalbis[(perfluoroalkyl)sulfonyl]imide; supported Lewis acid; catalysis; nitration;

D O I：

10.1016/j.apcata.2005.08.014

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

MCM-41-supported metal bis[(perfluoroalkyl)sulfonyl]imides were synthesized and characterized by FTIR, pyridine-FTIR, XRD, SEM, TGDTA and N-2-adsorption techniques. The heterogeneous catalysts were employed for nitration of aromatic compounds with 1 eq. of 65 wt% nitric acid in the liquid phase. The results showed that MCM-41-supported metal bis[(perfluoroalkyl)sulfonyl]imides were highly effective and could be recycled at least five times without substantial loss of catalytic activity. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：170 / 176

页数：7

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