Sintering of MnZn-ferrite powders prepared by hydrothermal reactions between oxides

被引:20
|
作者
Makovec, D [1 ]
Drofenik, M
Znidarsic, A
机构
[1] Jozef Stefan Inst, Dept Ceram, Ljubljana, Slovenia
[2] ISKRA Feriti, Ljubljana, Slovenia
关键词
ferrites; porosity; powders : chemical preparation; sintering; soft magnets;
D O I
10.1016/S0955-2219(01)00148-0
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The sintering of ferrite powders prepared by a hydrothermal treatment of starting oxides was studied in comparison with conventional pre-sintered powders. Two hydrothermal powders were prepared, one with a similar degree of conversion into spinel products as the pre-sintered powder but with a larger specific surface, and the other with a lower specific surface area and a high degree of conversion into MnZnFe2O4. In the first powder, non-homogeneity caused primarily by the agglomeration of the Mn-rich particles (Mn3O4 and ZnMn2O4) resulted in the formation of Kirkendall porosity, which significantly influenced the densification. process. (C) 2001 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:1945 / 1949
页数:5
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