Identification and Quantitation of the Bioactive Components in Osmanthus fragrans Fruits by HPLC-ESI-MS/MS

被引：29
|
作者：
Liao, Xiaoyan [1 ,2 ,3 ]
Hu, Fangli [1 ,2 ]
Chen, Zilin [1 ,2 ,3 ]
机构：
[1] Minist Educ, Key Lab Combinatorial Biosynth & Drug Discovery, Wuhan 430071, Hubei, Peoples R China
[2] Wuhan Univ, Sch Pharmaceut Sci, Wuhan 430071, Hubei, Peoples R China
[3] Chinese Acad Sci, State Key Lab Transducer Technol, Beijing 10080, Peoples R China
来源：
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY | 2018年 / 66卷 / 01期
基金：
中国国家自然科学基金;
关键词：
Osmanthus fragrans fruits; HPLC-ESI-MS/MS; identification; quantitation; bioactive components; phenylethanoid glycosides; TANDEM MASS-SPECTROMETRY; ANTIOXIDANT ACTIVITY; FRAXINUS-EXCELSIOR; LOUR; FLOWERS; URSOLIC ACID; GLYCOSIDE; DIFFERENTIATION; SECOIRIDOIDS; METABOLITE; ACTEOSIDE;
D O I：
10.1021/acs.jafc.7b05560
中图分类号：
S [农业科学];
学科分类号：
09 ;
摘要：
Information on the chemical composition of Osmanthus fragrans fruits is still limited because there are many compounds present in low concentrations in the plant. In this work, the bioactive components in O. fragrans fruit extract were investigated by a new high-performance liquid chromatography electrospray ionization tandem mass spectrometry method, which allows sensitive analysis both in identification and quantitation. A total of 28 compounds were tentatively identified, and 16 components were discovered in O. fragrans fruits for the first time. The validated quantitative methods for the determination of the bioactive components were subsequently applied to analyze batches of O. fragrans fruits from different cultivars, which is beneficial for the comprehensive utilization of O. fragrans fruits.
引用
收藏
页码：359 / 367
页数：9
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