3-Chloro-6-[2-(cyclopentylidene)hydrazin-1-yl]pyridazine

被引：1
|
作者：
Ather, Abdul Qayyum [2 ,3 ]
Tahir, M. Nawaz [1 ]
Khan, Misbahul Ain [2 ]
Athar, Muhammad Makshoof [4 ]
机构：
[1] Univ Sargodha, Dept Phys, Sargodha, Pakistan
[2] Islamia Univ, Dept Chem, Bahawalpur, Pakistan
[3] Appl Chem Res Ctr, Lahore 54600, Pakistan
[4] Univ Punjab, Inst Chem, Lahore, Pakistan
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
D O I：
10.1107/S1600536811011342
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title compound, C9H11ClN4, contains two virtually planar molecules that differ in conformation about the bond connecting the hydrazine and pyridazine units. The 3-chloro-6-hydrazinylpyridazine and cyclopentane groups are oriented at dihedral angles of 4.5 (3) and 8.8 (4)degrees in the two molecules. In the crystal, the molecules form a one dimensional polymeric structure extending along the a axis via N-H...N hydrogen bonds. The crystal stucired was an inversion twin [ratio of the twin domains = 0.73 (9):0.27 (9)].
引用
收藏
页码：O1020 / U1776
页数：11
相关论文
共 50 条
  • [41] Intramolecular hydrogen bonding between 2-cyanoguanidine and 3-chloro-6-(pyrazol-1-yl)pyridazines in copper(II) complexes
    Blake, AJ
    Hubberstey, P
    Li, WS
    Russell, CE
    Smith, BJ
    Wraith, LD
    JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1998, (04): : 647 - 655
  • [42] N-(2-(1H-indol-3-yl)ethyl)-2-(6-chloro-9H-carbazol-2-yl)propanamide
    Manolov, Stanimir
    Ivanov, Iliyan
    Bojilov, Dimitar
    MOLBANK, 2020, 2020 (04)
  • [43] Synthesis, crystal structure and Hirshfeld surface analysis of 5-[2-(dicyanomethylidene)hydrazin-1-yl]-2,4,6-triiodoisophthalic acid ethanol monosolvate
    Aliyeva, Fargana S.
    Mammadova, Gunay Z.
    Akkurt, Mehmet
    Celikesi, Sevim Turktekin
    Bhattarai, Ajaya
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2023, 79 : 795 - +
  • [44] (Z)-2-[(E)-2-(1-Benzothiophen-3-yl-methylidene)hydrazin-1-ylidene]-1,2-diphenylethanone
    Pekdemir, Merve
    Isik, Samil
    Gumus, Sumeyye
    Agar, Erbil
    Soylu, Mustafa Serkan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02579 - +
  • [45] PYRIDAZINES .1. NOVEL INTRAMOLECULAR CYCLOADDITION OF 3-CHLORO-6-(2-ALLYLPHENOXY)PYRIDAZINES
    JOJIMA, T
    TAKESHIB.H
    KONOTSUN.T
    CHEMICAL & PHARMACEUTICAL BULLETIN, 1972, 20 (10) : 2191 - +
  • [46] Diaquabis(N,N-diethylpyridine-3-carboxamide-κN1)bis{4-[ 2-(2,4-dioxopentan-3-ylidene)hydrazin-1-yl]benzoato-κO}copper(II)
    Alieva, Rafiqa A.
    Mardanova, Vusala I.
    Chyraqov, Famil M.
    Gurbanov, Atash V.
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : M127 - U473
  • [47] 1-{6-Chloro-2-[(2-chloro-6-methylquinolin-3-yl)methoxy]-4-phenylquinolin-3-yl}ethanone
    Khan, F. Nawaz
    Hathwar, Venkatesha R.
    Kumar, Rajesh
    Kushwaha, Atul Kumar
    Akkurt, Mehmet
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1693 - U488
  • [48] 2-(4-Chloro-1H-indol-3-yl)acetonitrile
    Pan, Mei-Ling
    Li, Xiang
    Luo, Yang-Hui
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [49] 2-Chloro-3-[(E)-(hydrazin-1-ylidene)methyl]-6-methoxyquinoline
    Bouacida, Sofiane
    Bouraiou, Abdelmalek
    Benhamoud, Nassima
    Roisnel, Thierry
    Belfaitah, Ali
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1548 - +
  • [50] 2-{[2-(2-Hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]methyl}-6-methoxyphenol
    Lu, Rong
    Wang, Wenxia
    Lu, Xingqiang
    Zhao, Shunsheng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2702 - +
12345