Data on validation using accuracy profile of HPLC-UV method

被引：3
|
作者：
Ibrahim, Ahmed M. [1 ]
Hendawy, Hassan A. M. [1 ]
Hassan, Wafaa S. [2 ]
Shalaby, Abdalla [2 ]
El-sayed, Heba M. [2 ]
机构：
[1] Natl Org Drug Control & Res, POB 29, Cairo, Egypt
[2] Zagazig Univ, Fac Pharm, Dept Analyt Chem, Zagazig, Egypt
来源：
DATA IN BRIEF | 2019年 / 24卷
关键词：
Accuracy profile; HPLC; Ascorbic acid; Paracetamol; Guaifenesin;
D O I：
10.1016/j.dib.2019.103877
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
The data presented are related to the article entitled "Six Sigma quality approach for HPLC-UV method optimization" Ibrahim et al., 2019. The raw data of HPLC analysis of ascorbic acid (AS), paracetamol (PA) and guaifenesin (GU) are presented. Calibration standards were prepared at six concentrations levels (25%, 50%, 75%, 100%, 125% and 150%) each day and measured in triplicate. Validation standards were prepared at four concentration levels (25%, 60%, 100% and 150%) each day and measured in quintet. Three different series were used for method validation and prepared at the rate of one series per day. (C) 2019 The Authors. Published by Elsevier Inc.
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页数：4
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