New synthesis of 5-cyano-1,2,4-thiadiazoles

被引:5
|
作者
Iwakawa, T [1 ]
Murabayashi, A [1 ]
机构
[1] Shionogi & Co Ltd, Aburahi Labs, Shiga 5203423, Japan
关键词
D O I
10.3987/COM-98-8459
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Treatment of 4-chloro-5-(3-isoxazolylimino)-5H-1,2,3-dithiazoles with piperidine in dichloromethane gave 5-cyano-1,2,4-thiadiazoles (51.8 %-92.1 % yield).
引用
收藏
页码:811 / 819
页数:9
相关论文
共 50 条
  • [31] Synthesis and spectroscopic properties of 15N-labelled 1,2,4-thiadiazoles
    Pavlik, JW
    Changtong, C
    Tantayanon, S
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2002, 39 (01) : 237 - 239
  • [32] An Expeditious Ultrasound-Initiated Green Synthesis of 1,2,4-Thiadiazoles in Water
    Chauhan, Swati
    Verma, Pratibha
    Mishra, Ankush
    Srivastava, Vandana
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2020, 56 (01) : 123 - 126
  • [33] SYNTHESIS OF FUSED 1,2,4-THIADIAZOLES FROM 5-CHLORO-1,2,4-THIADIAZOL-3(2H)-ONES
    LABBE, G
    BUELENS, J
    DEHAEN, W
    TOPPET, S
    FENEAUDUPONT, J
    DECLERCQ, JP
    TETRAHEDRON, 1994, 50 (24) : 7019 - 7028
  • [34] Synthesis of substituted 1,2,4-triazoles and 1,3,4-thiadiazoles
    Hovsepian, TR
    Dilanian, ER
    Engoian, AP
    Melik-Ohanjanian, RG
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2004, (09): : 1377 - 1381
  • [35] An Expeditious Ultrasound-Initiated Green Synthesis of 1,2,4-Thiadiazoles in Water
    Swati Chauhan
    Pratibha Verma
    Ankush Mishra
    Vandana Srivastava
    Chemistry of Heterocyclic Compounds, 2020, 56 : 123 - 126
  • [36] Synthesis of substituted 1,2,4-triazoles and 1,3,4-thiadiazoles
    Hovsepian T.R.
    Dilanian E.R.
    Engoyan A.P.
    Melik-Ohanjanian R.G.
    Chemistry of Heterocyclic Compounds, 2004, 40 (09) : 1194 - 1198
  • [37] Novel 1,2,4-Thiadiazoles with an NO-Producing Fragment
    Serkov, I. V.
    Proshin, A. N.
    Petrova, L. N.
    Bachurin, S. O.
    DOKLADY CHEMISTRY, 2010, 435 : 311 - 313
  • [38] MASS-SPECTRA OF SOME 1,2,4-THIADIAZOLES
    POTTS, KT
    ARMBRUST.R
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1972, 9 (03) : 651 - &
  • [39] Photochemistry of (4′-substituted)phenyl-1,2,4-thiadiazoles
    Changtong, Chuchawin
    Pavlik, James W.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2005, 230 : U3372 - U3373
  • [40] Novel 1,2,4-thiadiazoles with an NO-producing fragment
    I. V. Serkov
    A. N. Proshin
    L. N. Petrova
    S. O. Bachurin
    Doklady Chemistry, 2010, 435 : 311 - 313