Synthesis of a forsterite powder by combined ball milling and thermal treatment

被引：68

作者：

Kosanovic, C

Stubicar, N

Tomasic, N

Bermanec, V

Stubicar, M

机构：

[1] Rudjer Boskovic Inst, HR-10000 Zagreb, Croatia

[2] Univ Zagreb, Fac Sci, Dept Chem, HR-10001 Zagreb, Croatia

[3] Univ Zagreb, Fac Sci, Inst Mineral & Petrog, HR-10000 Zagreb, Croatia

[4] Univ Zagreb, Fac Sci, Dept Phys, HR-10002 Zagreb, Croatia

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2005年 / 389卷 / 1-2期

关键词：

oxide ceramics; forsterite; high-energy ball milling; solid state transformation; X-ray diffraction; FT-IR spectroscopy; DSC;

D O I：

10.1016/j.jallcom.2004.08.015

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Using powder mixtures of NH4-exchanged zeolite A and MgO as starting materials, forsterite was obtained as the final phase. The preparation procedure consisted of two steps: high-energy ball milling and thermal treatment. Ball milling was applied to amorphise NH4-exchanged zeolite A, to reduce the particle size of MgO, and to mix these two components. Thermal treatment of the milled mixture above 900degreesC for 3 h yielded forsterite as a dominant phase. Small amount of minor phases appeared beside forsterite. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：306 / 309

页数：4

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