A New Type of Bismuth Electrode for Electrochemical Stripping Analysis Based on the Ammonium Tetrafluorobismuthate Bulk-Modified Carbon Paste

被引：41
|
作者：
Sopha, Hanna [1 ]
Baldrianova, Lucie [2 ]
Tesarova, Eva [2 ]
Grinciene, Giedre [3 ]
Weidlich, Tomas [4 ]
Svancara, Ivan [2 ]
Hocevar, Samo B. [1 ]
机构：
[1] Natl Inst Chem, Analyt Chem Lab, SI-1000 Ljubljana, Slovenia
[2] Univ Pardubice, Dept Analyt Chem, Fac Chem Technol, CZ-53210 Pardubice, Czech Republic
[3] Inst Chem, Dept Catalysis, LT-01108 Vilnius, Lithuania
[4] Univ Pardubice, Inst Environm Protect, Fac Chem Technol, CZ-53210 Pardubice, Czech Republic
来源：
ELECTROANALYSIS | 2010年 / 22卷 / 13期
关键词：
Ammonium tetrafluorobismuthate; Carbon paste electrode; Anodic stripping voltammetry; Cadmium; Lead; FILM ELECTRODE; VOLTAMMETRY; ELECTROANALYSIS; CHEMISTRY; LIQUID;
D O I：
10.1002/elan.201070010
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A carbon paste electrode bulk-modified with ammonium tetrafluorobismuthate (BiF4-CPE) was developed and examined in the anodic stripping voltatnmetric mode for measurement of selected trace heavy metals. The BiF4-CPE has revealed a favorable performance in more acidic solutions (pH 0.5-2.5) in the presence of dissolved oxygen for Cd(II) and Pb(II) as model metal ions at the low mu g L-1 concentration level. In comparison with the bismuth-oxide bulk-modified carbon paste electrode and the other two bismuth film-plated carbonaceous substrate electrodes examined, the BiF4-CPE proved to be another attractive variant of the environmentally friendly bismuth-based electrodes, particularly convenient for analysis of acidified water samples.
引用
收藏
页码：1489 / 1493
页数：5
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