Synthesis of Ca(OH)2 nanoparticles by wet chemical method

被引:31
|
作者
Roy, A. [1 ]
Bhattacharya, J. [1 ]
机构
[1] Indian Inst Technol, Dept Min Engn, Kharagpur 721302, W Bengal, India
来源
MICRO & NANO LETTERS | 2010年 / 5卷 / 02期
关键词
IN-OIL MICROEMULSIONS; COLLOIDAL PARTICLES; REVERSE MICELLES; HYDROXIDE; WATER; HYDROLYSIS; SIZE; PBS;
D O I
10.1049/mnl.2010.0020
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
This Letter reports a process of preparation and characterisation of Ca(OH)(2) nanoparticles without using any surfactant. Ca(OH)(2) is frequently used as precipitant, catalyst, paint, toxic-waste remediation agent, adsorbent and so on. To prepare stable Ca(OH)(2) nanoparticles, a simple hydrolysis method was applied using Ca(NO3)(2)center dot 4H(2)O as the precursor, aqueous NaOH as the precipitant and ethane-1,2-diol (ED) as the medium. The nanoparticles were characterised by X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, high-resolution transmission electron microscope (HRTEM) and field emission scanning electron microscopy (FESEM). The results showed that the nanoparticles are of about 47 nm in diameter and P3m1 hexagonal structure. The method is simple and effective so that nanoparticles are stable up to 45 days, confirmed by the XRD pattern.
引用
收藏
页码:131 / 134
页数:4
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