Phase composition and physical properties of high-carbon Fe-C films

被引:0
|
作者
Shpak, A. P. [1 ]
Bashev, V. F. [2 ]
Brekharya, G. P. [3 ]
BoL'Shakov, V. I. [4 ]
Beletska, O. E. [2 ,4 ]
Dotsenko, F. F. [2 ]
Ryabtsev, S. I. [2 ]
机构
[1] NASU, GV Kurdyumov Inst Met Physi, UA-03680 Kiev 142, Ukraine
[2] Denpropetrovsk Natl Univ, UA-49050 Dnepropetrovsk, Ukraine
[3] Dneprodzerzhinsk State Tech Univ, UA-59118 Dnepropetrovsk, Ukraine
[4] Pridneprovsk State Academy of Bldg and Archititec, UA-49005 Dnepropetrovsk, Ukraine
来源
METALLOFIZIKA I NOVEISHIE TEKHNOLOGII | 2007年 / 29卷 / 10期
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中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The formation conditions for metastable structures and phase transformations during the heat treatment of high-carbon Fe-C films (20-84 at.% C) are studied by X-ray analysis, electron microscopy, measuring of the relative electrical resistance, and magnetic measuring. The films of a Fe-C system are fabricated by modernized three-electrode ion-plasma sputtering. As shown, the films with 20-31% C in. an initial state have an X-ray amorphous structure; the films with 40-60% C have an amorphous structure. The transformation of a film structure from an amorphous state to an equilibrium one during an annealing occurs through the formation and subsequent decomposition of the intermediate metastable h.c.p. phase with a variable content. The causes and mechanism of high values of magnetic-rigidity characteristics in obtained high-carbon Fe-C films at optimal compositions and heat-treatment regimes are suggested. The precise values of temperature coefficient of resistance are determined for Fe-C films.
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页码:1369 / 1381
页数:13
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