Bis(dimethylformamide-2κO)dipyridine-1κN,3κN-bis(μ-2′-salicylbenzohydrazidato)-1κ3O,N,O′:2κ2N,O";2κ2N,O":3κ3O,N,O′-trinickel(II) dimethylformamide disolvate hemihydrate

被引：10
|
作者：
Yang, MX [1 ]
Lin, S [1 ]
机构：
[1] Fujian Normal Univ, Coll Chem & Mat Sci, Fujian 350007, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2005年 / 61卷
关键词：
D O I：
10.1107/S1600536805013875
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the trinuclear nickel(II) complex of the title compound, [Ni-3(C30H20N4O6)(2)(C5H5N)(2)(C2H6NO)(2)](.)2C(3)H(7)NO(.)0.5H(2)O, the central Ni2+ ion is located on an inversion centre. This Ni2+ ion has a distorted octahedral coordination geometry involving two N and two O atoms from the 2 '-salicylbenzohydrazidate ligands in the equatorial plane and two N atoms from two dimethylformamide molecules in the axial positions. The inversion-related outer Ni2+ ions, separated by 9.3038 (7) angstrom, have square-planar coordination environments.
引用
收藏
页码：M1095 / M1096
页数：2
相关论文
共 50 条
  • [21] Bis[μ2-N,N′-bis(2-oxidobenzyl)propane-1,3-diamine]-1κ4O,N,N′,O′:2κ2O,O′:2κ2O,O′:3κ4O,N,N′,O′-bis(N,N′-dimethylformamide)1κO,3κO-di-μ2acetato-1:2κ2O: O′;2:3κ2O:;O′dinickel(II)zinc(II)
    Yildirim, Leyla Tatar
    Ergun, Uemit
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : m2424 - m2425
  • [22] Di-μ-benzoato-κ3O,O′:O;κ3O:O,O′-bis[(acetato-κO)(1,10-phenanthroline-κ2N,N′)lead(II)] dihydrate
    Gao, Junli
    Xuan, Xiaopeng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M900 - U731
  • [23] Di-μ-acesulfamato-κ3N,O:O;κ3O:N,O-bis[(acesulfamato-κ2N,O)bis(3-methylpyridine)cadmium(II)]
    Sahin, Zarife Sibel
    Icbudak, Hasan
    Isik, Samil
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2009, 65 : M463 - M465
  • [24] Tetrakis(μ2-3,4-dimethoxyphenylacetato)-κ3O,O′:O′;κ3O:O:O′;κ2O:O′;κ2O:O′-bis[(3,4-dimethoxyphenylacetato-κ2O,O′)(1,10-phenanthroline-κ2N,N)thulium(III)]
    Liu, Jia-Lu
    Li, Hua-Qiong
    Zhao, Guo-Liang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M9 - U215
  • [25] catena-Poly[[lead(II)-bis(μ2-quinolin-8-olato)-κ3N,O:O;κ3O:N,O] N,N-dimethylformamide hemisolvate]
    Ghaemi, Akbar
    Dadkhah, Zohreh
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : M210 - U1171
  • [26] Tetra-μ-acetato-κ4O:O′;κ3O,O′:O;κ3O":O,O′-bis[(acetato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)holmium(III)]
    Hu, Xue-Lei
    Qiu, Li
    Sun, Wen-Bing
    Chen, Zhong
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M3213 - M3214
  • [27] Tetra-μ-acetato-κ4O:O′;κ3O,O′:O′;κ3O:O,O′-bis[(acetato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)europium(III)]
    Liu, Wen-Jing
    Li, Zhao-Yang
    Wei, Zhi-Qiang
    Yue, Shan-Tang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M606 - U157
  • [28] Tetra-μ-benzoato-κ4O:O′;κ3O:O,O′;κ3O,O′:O′-bis[(benzoato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)terbium(III)] benzoic acid disolvate
    Ooi, Ping Howe
    Teoh, Siang Guan
    Yeap, Chin Sing
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M644 - U479
  • [29] Tetra-μ-benzoato-κ4O:O′;κ3O:O,O';κ3O,O′:O'-bis[(benzoato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)europium(III)] benzoic acid disolvate
    Ooi, Ping Howe
    Teoh, Siang Guan
    Yeap, Chin Sing
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M597 - U1166
  • [30] Tetra-μ-benzoato-κ4O:O′;κ3O:O,O′;κ3O,O′:O′-bis[(benzoato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)neodymium(III)]
    Ooi, Ping Howe
    Teoh, Siang Guan
    Goh, Jia Hao
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M221 - U1270
12345