A simple preparation procedure for the synthesis of sodium hexaniobate nanorods

被引：13
|
作者：
Lin, CH
Lee, CH
Chao, JH
Huang, YM
Chang, HW
Kuo, CY
Hsu, CW
机构：
[1] Natl Changhua Univ Educ, Dept Chem, Changhua 50058, Taiwan
[2] Natl Tsing Hua Univ, Dept Engn & Syst Sci, Hsinchu 300, Taiwan
[3] Natl Tsing Hua Univ, Nucl Sci & Technol Dev Ctr, Hsinchu 300, Taiwan
来源：
MATERIALS CHEMISTRY AND PHYSICS | 2005年 / 92卷 / 01期
关键词：
sodium hexaniobate; nanorods; hydrothermal; Nb2O5;
D O I：
10.1016/j.matchemphys.2005.01.003
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A simple hydrothermal method was used to synthesize crystalline sodium hexamobate nanorods of high purity in gram quantity by treating Nb2O5 powder in 10M NaOH at 150 degrees C without utilizing template molecules. The molecular composition of such material was identified as Na6HNb6O19.2H(2)O. SEM revealed that the majority of these hexamobate rods had a diameter distribution of 200-450nm and a length distribution of 40-60 mu m, though finer rods with a diameter of 50-100 nm could also be found in the product mixture. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码：128 / 133
页数：6
相关论文
共 50 条
  • [11] A simple method for the synthesis of silicon carbide nanorods
    Kholmanov, IN
    Kharlamov, A
    Barborini, E
    Lenardi, C
    Li Bassi, A
    Bottani, CE
    Ducati, C
    Maffi, S
    Kirillova, NV
    Milani, P
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2002, 2 (05) : 453 - 456
  • [12] Synthesis of sodium tantalate nanorods by alkalide reduction
    Nelson, JA
    Wagner, MJ
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2003, 125 (02) : 332 - 333
  • [13] Synthesis of sodium tantalate nanorods by alkalide reduction
    1600, American Chemical Society (125):
  • [14] A simple and convenient catalytic procedure for the preparation of dithioacetals
    Graham, AE
    SYNTHETIC COMMUNICATIONS, 1999, 29 (04) : 697 - 703
  • [15] A SIMPLE AND INEXPENSIVE PROCEDURE FOR THE PREPARATION OF (DICHLOROIODO)ARENES
    KOYUNCU, D
    MCKILLOP, A
    MCLAREN, L
    JOURNAL OF CHEMICAL RESEARCH-S, 1990, (01): : 21 - 21
  • [16] A SIMPLE PROCEDURE FOR THE PREPARATION OF METHYL-ESTERS
    RAO, AVR
    DESHMUKH, MN
    SIVADASAN, L
    CHEMISTRY & INDUSTRY, 1981, (05) : 164 - 164
  • [17] A SIMPLE PROCEDURE FOR THE PREPARATION OF L-HEXOSES
    HAUSER, FM
    ELLENBERGER, SR
    ELLENBERGER, WP
    TETRAHEDRON LETTERS, 1988, 29 (39) : 4939 - 4942
  • [18] A SIMPLE PROCEDURE FOR PREPARATION OF REDUCED CYTOCHROME C
    HORTON, AA
    ANALYTICAL BIOCHEMISTRY, 1968, 23 (02) : 334 - &
  • [19] A SIMPLE PROCEDURE FOR THE PREPARATION OF LIPOPOLYSACCHARIDE FOR THE PRODUCTION OF ANTISERA
    CHART, H
    ROWE, B
    LETTERS IN APPLIED MICROBIOLOGY, 1992, 14 (06) : 263 - 265
  • [20] A SIMPLE PROCEDURE FOR PREPARATION OF REV-LIPOSOMES
    ARNHOLD, J
    DEEV, AI
    PHARMAZIE, 1985, 40 (11): : 808 - 809
12345