A simple three-component synthesis of spiro-pyran derivatives

被引:19
|
作者
He, Yi [1 ]
Guo, Hongyun [1 ]
Tian, Jinjin [1 ]
机构
[1] Zhejiang Univ Technol, Coll Chem Engn & Mat, Hangzhou 310014, Zhejiang, Peoples R China
关键词
one-pot; spiro-pyran derivatives; NaHCO3;
D O I
10.3184/174751911X13149692358913
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A series of spiro-pyran derivatives have been synthesised by a three-component reaction of ninhydrin or acenaphthenequinone, malononitrile and 1,3-dicarbonyl compounds such as cyclohexane-1,3-dione, dimedone and barbituaric acid in ethanol with NaHCO3 as the catalyst. This method has the advantages of easy work-up, mild reaction condition, high yields and it is cheap.
引用
收藏
页码:528 / 530
页数:3
相关论文
共 50 条
  • [41] Three-component 1,3-dipolar cycloaddition reactions in synthesis of spiro[pyrrolidine-2,3′-oxindoline] derivatives
    El-Ahl, AAS
    HETEROATOM CHEMISTRY, 2002, 13 (04) : 324 - 329
  • [42] Simple Synthesis of Polyfunctionalized Indoline-Spiro Fused Pyran Derivatives via an Aqueous Multicomponent Reaction
    Dolati, Hadi
    Habibi, Azizollah
    Ayatollahi, Seyed Abdul Majid
    Mahdavi, Seyedeh Mahbobeh
    Valizadeh, Yousef
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 2016, 38 (03): : 517 - 523
  • [43] Preparation of poly(methyl methacrylate) photochromic microcapsules containing spiro-pyran by solvent volatilization
    Gao, Jian
    Dong, Jiansheng
    Yin, Yunjie
    JOURNAL OF PHOTOPOLYMER SCIENCE AND TECHNOLOGY, 2023, 36 (05) : 305 - 314
  • [44] Facile one pot microwave assisted solvent-free synthesis of novel spiro-fused pyran derivatives via the three-component condensation of ninhydrin with malononitrile and active methylene compounds
    Shaker, RM
    Mahmoud, AF
    Abdel-Latif, FF
    JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2005, 52 (03) : 563 - 567
  • [45] Potassium Phosphate Catalyzed a Rapid Three-Component Synthesis of Tetrahydrobenzo[b]pyran at Ambient Temperature
    D. M. Pore
    K. A. Undale
    B. B. Dongare
    U. V. Desai
    Catalysis Letters, 2009, 132 : 104 - 108
  • [46] Potassium Phosphate Catalyzed a Rapid Three-Component Synthesis of Tetrahydrobenzo[b]pyran at Ambient Temperature
    Pore, D. M.
    Undale, K. A.
    Dongare, B. B.
    Desai, U. V.
    CATALYSIS LETTERS, 2009, 132 (1-2) : 104 - 108
  • [47] A Three-Component Synthesis of Spiropyrrolines
    Sahoo, Kanchanbala
    Patra, Nityaprakash
    Dandela, Rambabu
    Thirupathi, Barla
    JOURNAL OF ORGANIC CHEMISTRY, 2024, 89 (08): : 5337 - 5352
  • [48] A simple and clean procedure for three-component synthesis of spirooxindoles in aqueous medium
    Zhu, Song-Lei
    Ji, Shun-Jun
    Zhang, Yong
    TETRAHEDRON, 2007, 63 (38) : 9365 - 9372
  • [49] Synthesis of functionalized 4H-pyran and cyclohexanone derivatives via three-component reactions of dimethyl acetonedicarboxylate, aromatic aldehydes, and malononitrile
    Heber, D
    Stoyanov, EV
    SYNTHESIS-STUTTGART, 2003, (02): : 227 - 232
  • [50] One-pot three-component synthesis of α-amino phosphonate derivatives
    Heydari, Akbar
    Arefi, Afsaneh
    CATALYSIS COMMUNICATIONS, 2007, 8 (07) : 1023 - 1026