Preparation of tributylborane from butyllithium and boron trifluoride etherate

被引：1
|
作者：
Wu, YK
Shen, X
机构：
[1] Chinese Acad Sci, Shanghai Inst Organ Chem, State Key Lab Bioorgan & Natl Prod Chem, Shanghai 200032, Peoples R China
[2] Chinese Acad Sci, Shanghai Inst Organ Chem, Shanghai Hong Kong Joint Lab Chem Synth, Shanghai 200032, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2001年 / 31卷 / 19期
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1081/SCC-100105665
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A convenient laboratory synthesis of tributylborane from commercially available n-butyllithium and boron trifluoride etherate is developed.
引用
收藏
页码：2939 / 2942
页数：4
相关论文
共 50 条
  • [31] Chain termination in polymerization of substituted oxetanes in the presence of boron trifluoride etherate
    A. E. Tarasov
    O. M. Ol’khova
    Ya. I. Estrin
    G. V. Lagodzinskaya
    E. R. Badamshina
    Yu. M. Mikhailov
    Polymer Science Series B, 2013, 55 : 116 - 121
  • [32] ELECTROPOLYMERIZATION OF CARBAZOLE IN MIXED ELECTROLYTE OF TETRAHYDROFURAN AND BORON TRIFLUORIDE DIETHYL ETHERATE
    Shen Yanyan
    Miao Huaming
    Xu Jingkun
    Zhang Honglin
    Lu Baoyang
    ACTA POLYMERICA SINICA, 2008, (11) : 1089 - 1095
  • [33] Electrochemical polymerization of fluorene halide in boron trifluoride diethyl etherate solution
    Chen Wen
    Fan Changli
    Zeng Liqiang
    Wang Xingcong
    Chu Qi
    Xu Jingkun
    ACTA POLYMERICA SINICA, 2008, (09): : 861 - 866
  • [34] AN IMPROVED PROCEDURE FOR THE ACYLATION OF PHENOLS USING BORON TRIFLUORIDE-ETHERATE
    MOHANTY, S
    GROVER, SK
    CURRENT SCIENCE, 1988, 57 (10): : 537 - 538
  • [35] Fluorination of aromatic compounds with xenon difluoride in the presence of boron trifluoride etherate
    Fedorov, A. E.
    Zubarev, A. A.
    Mortikov, V. Yu.
    Rodinovskaya, L. A.
    Shestopalov, A. M.
    RUSSIAN CHEMICAL BULLETIN, 2015, 64 (05) : 1049 - 1052
  • [36] HYDROGEN PEROXIDE-BORON TRIFLUORIDE ETHERATE, A NEW OXIDIZING AGENT
    MCCLURE, JD
    WILLIAMS, PH
    JOURNAL OF ORGANIC CHEMISTRY, 1962, 27 (01): : 24 - &
  • [37] REACTION OF THE GLUCOSE DERIVATIVES WITH DIAZOETHANE IN THE PRESENCE OF BORON-TRIFLUORIDE ETHERATE
    SEBYAKIN, YL
    VOLKOVA, LV
    EVSTIGNEEVA, RP
    ZHURNAL OBSHCHEI KHIMII, 1979, 49 (01): : 221 - 223
  • [38] FORMATION OF ETHERS FROM UNSATURATED ALIPHATIC-ALCOHOLS IN PRESENCE OF BORON-TRIFLUORIDE ETHERATE
    NAGAI, K
    NAKAYAMA, M
    HAYASHI, S
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1978, 51 (11) : 3273 - 3276
  • [39] REGIOSELECTIVE AND STEREOSELECTIVE CLEAVAGE OF EPOXIDES WITH CYANOBOROHYDRIDE AND BORON-TRIFLUORIDE ETHERATE
    HUTCHINS, RO
    TAFFER, IM
    BURGOYNE, W
    JOURNAL OF ORGANIC CHEMISTRY, 1981, 46 (25): : 5214 - 5215
  • [40] EFFECT OF BORON-TRIFLUORIDE ETHERATE ON PHOTOREARRANGEMENT OF N-BENZYLANILINES
    FURUKAWA, J
    OMURA, K
    CHEMISTRY LETTERS, 1973, (10) : 1111 - 1114
12345