Parametric Analysis of 1,1-Diethoxybutane Synthesis in Fixed-Bed Reactor and Distillation Column‡

被引:1
|
作者
Tikekar, Ketaki [1 ]
Singh, Kailash [1 ]
Upadhyaya, Sushant [1 ]
机构
[1] Malaviya Natl Inst Technol, Dept Chem Engn, JLN Marg, Jaipur 302017, Rajasthan, India
关键词
Aspen Plus simulations; Biofuel additives; 1; 1-Diethoxybutane; Distillation columns; Fixed-bed reactors; Parametric studies; CATION-EXCHANGE RESINS; ETHANOL; BATCH;
D O I
10.1002/ceat.202100489
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
A comparison of two processes of the synthesis of 1,1-diethoxybutane (DEB) based on parametric analysis using Aspen Plus simulation has been investigated. DEB is an acetal which is a promising bio-based additive for biofuels and their blends with conventional fuels. The thermodynamic limitations due to reversibility of the reaction can be overcome by continuously removing the by-product water. The simulation and a parametric study of two different synthesis processes of DEB using a catalytic fixed-bed reactor and distillation column are described. The process with three reactors and three separators in series showed better results with respect to reactor temperature, productivity of DEB, and stages of distillation column than the one with a single reactor and separator.
引用
收藏
页码:489 / 496
页数:8
相关论文
共 50 条
  • [21] Adsorptive Removal of Pentachlorophenol by Anthracophyllum discolor in a Fixed-Bed Column Reactor
    Rubilar, Olga
    Tortella, Gonzalo R.
    Cuevas, Raphael
    Cea, Mara
    Rodriguez-Couto, Susana
    Cristina Diez, Maria
    WATER AIR AND SOIL POLLUTION, 2012, 223 (05): : 2463 - 2472
  • [22] Adsorptive Removal of Pentachlorophenol by Anthracophyllum discolor in a Fixed-Bed Column Reactor
    Olga Rubilar
    Gonzalo R. Tortella
    Raphael Cuevas
    Mara Cea
    Susana Rodríguez-Couto
    María Cristina Diez
    Water, Air, & Soil Pollution, 2012, 223 : 2463 - 2472
  • [23] Exergy analysis of chromatographic separations in a fixed-bed column
    Maia, MLO
    Ottens, M
    van der Wielen, LAM
    INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2004, 43 (12) : 3183 - 3193
  • [24] An analysis of convective dispersion and reaction in the fixed-bed reactor
    Gunn, DJ
    INTERNATIONAL JOURNAL OF HEAT AND MASS TRANSFER, 2004, 47 (12-13) : 2861 - 2875
  • [25] EXCITABLE WAVES IN A FIXED-BED REACTOR - OBSERVATIONS AND ANALYSIS
    SHEINTUCH, M
    CHEMICAL ENGINEERING SCIENCE, 1990, 45 (08) : 2125 - 2132
  • [26] FIXED-BED REACTOR SUCCESSFUL IN FUELS FROM COAL SYNTHESIS
    不详
    OIL & GAS JOURNAL, 1992, 90 (03) : 53 - 56
  • [27] Modeling, simulation and control of a methanol synthesis fixed-bed reactor
    Shahrokhi, M
    Baghmisheh, GR
    CHEMICAL ENGINEERING SCIENCE, 2005, 60 (15) : 4275 - 4286
  • [28] Thermodynamic and kinetic studies for synthesis of the acetal (1,1-diethoxybutane) catalyzed by Amberlyst 47 ion-exchange resin
    Rahaman, Mehabub
    Graca, Nuno S.
    Pereira, Carla S. M.
    Rodrigues, Alirio E.
    CHEMICAL ENGINEERING JOURNAL, 2015, 264 : 258 - 267
  • [29] Thermodynamic and kinetic studies for synthesis of the acetal (1,1-diethoxybutane) catalyzed by Amberlyst 47 ion-exchange resin
    Rahaman, Mehabub
    Graça, Nuno S.
    Pereira, Carla S.M.
    Rodrigues, Alírio E.
    Chemical Engineering Journal, 2015, 264 : 258 - 267
  • [30] Experimental and simulation studies of TAME synthesis in a fixed-bed reactor
    Ferreira, Manuela V.
    Ribeiro, Ana M.
    Loureiro, Jose M.
    INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2007, 46 (04) : 1105 - 1113