N-(4-methylpyridin-2-yl)-5H-dibenzo[d,f][1,3]diazepine-6-carboxamide toluene hemisolvate

被引：5
|
作者：
Hodorowicz, Maciej [1 ]
Stadnicka, Katarzyna [1 ]
Trzewik, Bartosz [1 ]
Zaleska, Barbara [1 ]
机构：
[1] Jagiellonian Univ, Fac Chem, PL-30060 Krakow, Poland
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807042687
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C20H16N4O·0.5C7H8, crystallizes with half a toluene mol-ecule (disordered about a centre of inversion); the seven-membered diazepine ring adopts a twist-boat conformation. The structure features two intra-molecular (N - H⋯O and N - H⋯N) and one inter-molecular hydrogen bond. Additional inter-molecular π-π inter-actions (3.556-3.651 Å) give rise to a three-dimensional network in the crystal structure. © International Union of Crystallography 2007.
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收藏
页码：O4115 / U3660
页数：11
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