Structural characterization of nickel(II) tetraphenylporphyrin

被引：56
|
作者：
Maclean, AL
Foran, GJ
Kennedy, BJ
Turner, P
Hambley, TW
机构：
[1] UNIV SYDNEY,SCH CHEM,SYDNEY,NSW 2006,AUSTRALIA
[2] AUSTRALIAN NUCL SCI & TECHNOL ORG,MENAI,NSW 2234,AUSTRALIA
来源：
AUSTRALIAN JOURNAL OF CHEMISTRY | 1996年 / 49卷 / 12期
关键词：
D O I：
10.1071/CH9961273
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The structure of 5,10,15,20-tetraphenylporphinatonickel(II) ([Ni(tpp)]) has been studied by both X-ray diffraction (powder and single-crystal methods) and EXAFS. The bond lengths obtained from analysis of the EXAFS agree, within standard deviations, with those obtained from the X-ray diffraction studies. The Ni-N bond length of 1.93(1) Angstrom agrees especially well with the value of 1.931(2) Angstrom obtained from the single-crystal analysis. The powder X-ray diffraction pattern, collected by using synchrotron radiation, is presented.
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收藏
页码：1273 / 1278
页数：6
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