Preparation of monolithic silica columns for high-performance liquid chromatography

被引：204
|
作者：
Nunez, Oscar [1 ,2 ]
Nakanishi, Kazuki [3 ]
Tanaka, Nobuo [2 ]
机构：
[1] Univ Barcelona, Fac Chem, Dept Analyt Chem, E-08028 Barcelona, Spain
[2] Kyoto Inst Technol, Grad Sch Sci & Technol, Dept Biomol Engn, Sakyo Ku, Kyoto 6068585, Japan
[3] Kyoto Univ, Grad Sch Sci, Dept Chem, Sakyo Ku, Kyoto 6068502, Japan
来源：
JOURNAL OF CHROMATOGRAPHY A | 2008年 / 1191卷 / 1-2期
基金：
日本学术振兴会;
关键词：
monolithic silica columns; reversed-phase; polymerization; chemical modification; HPLC; HILIC; ion-exchange; chiral; stationary phase;
D O I：
10.1016/j.chroma.2008.02.029
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Preparation methods of monolithic silica columns for HPLC including the surface modification were reviewed. Chemical modification methods recently reported to obtain stationary phases for reversed-phase (RP), chiral, ion-exchange, and hydrophilic interaction chromatography (HILIC) separations were discussed. Recent results related to preparation methods of monolithic silica were also covered. The characteristics and properties of silica monoliths and some applications of monolithic silica columns for different analytical and bioanalytical fields will be commented. (c) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码：231 / 252
页数：22
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