One-pot preparation of fluorinated α-aminoalkyl phosphonates under microwave irradiation and solvent-free conditions

被引：13
|
作者：
Lv, Xiao-yong
Zhang, Jian-min
Xing, Chun-hui
Du, Wei-qiong [1 ]
Zhu, Shi-zheng
机构：
[1] Shanghai Univ, Sch Sci, Dept Chem, Shanghai, Peoples R China
[2] Chinese Acad Sci, Shanghai Inst Organ Chem, Key Lab Organofluorine Chem, Shanghai, Peoples R China
来源：
SYNTHETIC COMMUNICATIONS | 2007年 / 37卷 / 4-6期
基金：
中国国家自然科学基金;
关键词：
alpha-aminoalkyl phosphonates; anilines; fluorinated aldehydes; microwave; solvent free;
D O I：
10.1080/00397910601131411
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A facile one-pot method has been developed for the synthesis of fluorine-containing a-amino phosphonates in good yields by a three-component reaction of fluorinated aromatic aldehydes, anilines, and diethyl phosphate in the presence of a silica-gel support under microwave irradiation within 10min. All new compounds are fully characterized by spectral methods and elemental analysis.
引用
收藏
页码：743 / 757
页数：15
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