Control of plantwide reactive distillation processes: Hydrolysis, transesterification and two-stage esterification

被引：14

作者：

Hung, Shih-Bo ^{[2
]}

Chen, Jyun-Hong ^{[1
]}

Lin, Yu-Der ^{[1
]}

Huang, Hsiao-Ping ^{[1
]}

Lee, Ming-Jer ^{[2
]}

Ward, Jeffrey D. ^{[1
]}

Yu, Cheng-Ching ^{[1
]}

机构：

[1] Natl Taiwan Univ, Dept Chem Eng, Taipei 10617, Taiwan

[2] Natl Taiwan Univ Sci & Technol, Dept Chem Eng, Taipei 10607, Taiwan

来源：

JOURNAL OF THE TAIWAN INSTITUTE OF CHEMICAL ENGINEERS | 2010年 / 41卷 / 04期

关键词：

Reactive distillation; Plantwide control; Hydrolysis; Transesterification; Adipic acid; METHYL ACETATE; COUPLED REACTOR/COLUMN; MULTIVARIABLE SYSTEMS; CHEMICAL-EQUILIBRIUM; LIQUID-MIXTURES; BUTYL ACETATE; DESIGN; METHANOL; COLUMN; ALTERNATIVES;

D O I：

10.1016/j.jtice.2010.03.021

中图分类号：

TQ [化学工业];

学科分类号：

0817 ;

摘要：

General design principles for controlling plantwide reactive distillation processes are developed in this work. Three cases of plantwide RD processes with large recycle flow rates are used to illustrate the application of the design principals. The cases are hydrolysis of methyl acetate, transesterification of methyl acetate and esterification of adipic acid. The design principles produce workable control structures for the three systems. Temperature and temperature-composition control structures can deal with the two major disturbances: changes in the feed flow rates and reactant composition. Results show that the control structures offer good robustness and acceptable dynamic performances. (C) 2010 Taiwan Institute of Chemical Engineers. Published by Elsevier B.V. All rights reserved.

引用

页码：382 / 402

页数：21

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