Thermal and photoluminescence properties of hydrated YPO4:Eu3+ nanowires

被引:62
|
作者
Di, Weihua
Zhao, Xiaoxia
Lu, Shaozhe
Wang, Xiaojun
Zhao, Haifeng
机构
[1] Chinese Acad Sci, Changchun Inst Opt Fine Mech & Phys, Key Lab Excited State Phys, Changchun 130033, Peoples R China
[2] Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
基金
中国国家自然科学基金;
关键词
rare earth; yttrium orthophosphate; hydrate; luminescence; thermal effect;
D O I
10.1016/j.jssc.2007.06.025
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
In this work, we used the solution precipitation route to synthesize Eu3+-doped YPO4 center dot nH(2)O nanowires. The structure, morphology, composition, thermal behavior, and photoluminescence of as-synthesized product were characterized by X-ray diffraction (XRD), thermogravimetric and differential thermal analysis (TG/DTA), energy-dispersive X-ray spectroscopy (EDS), Fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopic (FE-SEM) and photoluminescence (PL) spectra. The dependence of the structure, morphology, composition and luminescent properties on the thermal treatment was investigated. The results indicate that the aqueous synthesis has a better control on the structure, morphology, composition of the products, and that the heat treatment induces the transitions of the structure, composition, and luminescent properties. (c) 2007 Elsevier Inc. All rights reserved.
引用
收藏
页码:2478 / 2484
页数:7
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