Simple and Sensitive Method for Determination of Imidacloprid Residue in Soil and Water by HPLC

被引：19

作者：

Samnani, Prakash ^{[1
]}

Vishwakarma, Kamlesh ^{[2
]}

Pandey, S. Y. ^{[2
]}

机构：

[1] Maharaja Sayajirao Univ Baroda, Fac Sci, Dept Chem, Vadodara 390002, Gujarat, India

[2] Jai Res Fdn, Dept Chem, Valvada 396108, Gujarat, India

来源：

BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY | 2011年 / 86卷 / 05期

关键词：

HPLC; Imidacloprid; Residues; Soil; Water;

D O I：

10.1007/s00128-011-0245-8

中图分类号：

X [环境科学、安全科学];

学科分类号：

08 ; 0830 ;

摘要：

A rapid, sensitive and reliable HPLC method was developed and validated for the determination of imidacloprid residue in water at different pH and in soil. Quantification was performed by reversed phase HPLC system equipped with UV detector. The limit of quantification (LOQ) was found to be 0.02 mg/kg in soil and 0.02 mg/L in water. The limit of detection (LOD) was 0.006 mg/kg in soil and 0.006 mg/L in water. Recoveries for imidacloprid were 95.18%, 94.66%, 95.27% and 94.78% in black, red, sandy loam and clay soils, respectively. Recoveries for imidacloprid from water were 96.86%, 86.14%, and 92.34% at pH values of 4, 7, and 9, respectively.

引用

页码：554 / 558

页数：5

共 50 条

[11] Development of a Simple and Sensitive HPLC Method for the Determination of Rifaximin in Serum and its Application
Hossain, M. A.
Pervin, Rokeya
Park, Na-Hye
Kang, J. W.
Lee, K. J.
Suh, J. W.
Park, S. C.
INDIAN JOURNAL OF PHARMACEUTICAL SCIENCES, 2018, 80 (06) : 1108 - 1114
[12] Simple and sensitive RP-HPLC/RID method for the determination of triclofos sodium
Lakka, Narasimha Swamy
Praveen, B. N. V. V. D.
Chinta, Srinivasa Reddy
JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 2017, 94 (01) : 53 - 58
[13] Soil water diffusivity: A simple laboratory method for its determination
Villarreal, Rafael
Lozano, Luis A.
German Soracco, C.
Filgueira, Roberto R.
Sarli, Guillermo O.
WATER RESOURCES AND IRRIGATION MANAGEMENT-WRIM, 2016, 5 (01): : 15 - 21
[14] Development, validation and application of a sensitive analytical method for residue determination and dissipation of imidacloprid in sugarcane under tropical field condition
Ramasubramanian, T.
Paramasivam, M.
Nirmala, R.
ENVIRONMENTAL MONITORING AND ASSESSMENT, 2016, 188 (06)
[15] Development, validation and application of a sensitive analytical method for residue determination and dissipation of imidacloprid in sugarcane under tropical field condition
T. Ramasubramanian
M. Paramasivam
R. Nirmala
Environmental Monitoring and Assessment, 2016, 188
[16] A SIMPLE AND SENSITIVE HPLC METHOD FOR ANTIPYRINE IN PLASMA
SHEN, J
WANWIMOLRUK, S
JOURNAL OF LIQUID CHROMATOGRAPHY, 1991, 14 (14): : 2801 - 2808
[17] Development and validation of a simple and sensitive HPLC method for the determination of related substances in regorafenib tablets
Sijie Li
Mei Jiang
Minyue Li
Penghui Hu
Mingbo Xu
Chang Shu
Analytical Sciences, 2022, 38 : 591 - 599
[18] Development and validation of a simple and sensitive HPLC method for the determination of liquid form of therapeutic substances
Alkhamaisah, Suhaib Ibrahim
Younes, Kareem M.
Gaipov, Abduzhappar
Aljofan, Mohamad
ELECTRONIC JOURNAL OF GENERAL MEDICINE, 2019, 16 (06):
[19] SIMPLE, RAPID AND HIGH SENSITIVE HPLC METHOD FOR DETERMINATION OF PLATINUM(II) ANTINEOPLASTIC DRUG
BURDAROV, VI
MITEWA, MI
DOKLADI NA BOLGARSKATA AKADEMIYA NA NAUKITE, 1986, 39 (02): : 61 - 64
[20] Development and validation of a simple and sensitive HPLC method for the determination of related substances in regorafenib tablets
Li, Sijie
Jiang, Mei
Li, Minyue
Hu, Penghui
Xu, Mingbo
Shu, Chang
ANALYTICAL SCIENCES, 2022, 38 (03) : 591 - 599

← 1 2 3 4 5 →