Ultra-long Sialon nanobelts: large-scale synthesis via a pressure enhanced CVD process and photoluminescence characteristics

被引：26
|
作者：
Qin, Chunlin [1 ,2 ]
Wen, Guangwu [1 ,2 ]
Wang, Xinyu [1 ]
Song, Liang [1 ]
Huang, Xiaoxiao [2 ]
机构：
[1] Harbin Inst Technol, Sch Mat Sci & Engn, Harbin 150001, Peoples R China
[2] Harbin Inst Technol, Sch Mat Sci & Engn, Weihai 264209, Peoples R China
来源：
JOURNAL OF MATERIALS CHEMISTRY | 2011年 / 21卷 / 16期
基金：
中国国家自然科学基金;
关键词：
BETA-SIALONS; CERAMICS;
D O I：
10.1039/c0jm04247a
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Large quantities of core-shell structured Sialon nanobelts containing amorphous carbon in the shell were synthesized by pressure enhanced CVD at 1450 degrees C without a catalyst. The products are high-quality nano single-crystalline with a uniform morphology. The yield and aspect ratio are systematically controlled by changing the growth temperature and chamber pressure. The nanostructures were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), nitrogen adsorption-desorption isotherms and high-resolution transmission electron microscopy (HRTEM). A stepwise reaction model and luminescence characteristics were proposed based on the experimental results.
引用
收藏
页码：5985 / 5991
页数：7
相关论文
共 49 条
  • [21] Large-Scale Synthesis and Characterization of Very Long Silver Nanowires via Successive Multistep Growth
    Lee, Jin Hwan
    Lee, Phillip
    Lee, Dongjin
    Lee, Seung Seob
    Ko, Seung Hwan
    CRYSTAL GROWTH & DESIGN, 2012, 12 (11) : 5598 - 5605
  • [22] Synthesis and optical property of large-scale centimetres-long silicon carbide nanowires by catalyst-free CVD route under superatmospheric pressure conditions
    Lin, Liangwu
    NANOSCALE, 2011, 3 (04) : 1582 - 1591
  • [23] Large-scale synthesis of single-crystalline KNb3O8 nanobelts via a simple molten salt method
    Zhan, Z. Y.
    Xu, C. Y.
    Zhen, L.
    Wang, W. S.
    Shao, W. Z.
    CERAMICS INTERNATIONAL, 2010, 36 (02) : 679 - 682
  • [24] Large-scale synthesis of ultralong Bi2S3 nanoribbons via a solvothermal process
    Liu, ZP
    Peng, S
    Xie, Q
    Hu, ZK
    Yang, Y
    Zhang, SY
    Qian, YT
    ADVANCED MATERIALS, 2003, 15 (11) : 936 - +
  • [25] Large-scale synthesis of tungsten single-crystal microtubes via vapor-deposition process
    Wang, Shiliang
    He, Yuehui
    Liu, Xinli
    Zhang, Quan
    Zou, Jin
    Huang, Han
    Song, Min
    Huang, Baiyun
    Liu, C. T.
    Du, Yong
    JOURNAL OF CRYSTAL GROWTH, 2011, 316 (01) : 137 - 144
  • [26] Potential cost savings of large-scale blue hydrogen production via sorption-enhanced steam reforming process
    Udemu, Chinonyelum
    Font-Palma, Carolina
    ENERGY CONVERSION AND MANAGEMENT, 2024, 302
  • [27] Large-scale synthesis of crystalline tellurium nanowires with controlled-diameters via a hydrothermal-reduction process
    Xu, LQ
    Ding, YW
    Xi, GC
    Zhang, WQ
    Peng, YY
    Yu, WC
    Qian, YT
    CHEMISTRY LETTERS, 2004, 33 (05) : 592 - 593
  • [28] Facile large-scale synthesis of brain-like mesoporous silica nanocomposites via a selective etching process
    Chen, Yu
    Wang, Qihua
    Wang, Tingmei
    NANOSCALE, 2015, 7 (39) : 16442 - 16450
  • [29] Large-Scale Synthesis of Hierarchical Porous MOF Particles via a Gelation Process for High Areal Capacitance Supercapacitors
    Sun, Yujie
    Shi, Fei
    Wang, Bo
    Shi, Naien
    Ding, Zhen
    Xie, Linghai
    Jiang, Jiadong
    Han, Min
    NANOMATERIALS, 2023, 13 (10)
  • [30] Facile one-step hydrothermal synthesis of zinc vanadate nanomaterials enhanced via reduced graphene oxide for ultra-long life asymmetric supercapacitors
    Ankinapalli, Obula Reddy
    Krishna, B. N. Vamsi
    Yu, Jae Su
    JOURNAL OF POWER SOURCES, 2024, 591
12345