2-Aminobenzoato-κ2O,O′)(rac-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N",N"′)nickel(II) perchlorate monohydrate

被引：2

作者：

Ou, Guang-Chuan ^{[2
]}

Ng, Seik Weng ^{[1
]}

机构：

[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia

[2] Hunan Univ Sci & Engn, Dept Biol & Chem, Yongzhou 425100, Hunan, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷

关键词：

D O I：

10.1107/S1600536810037116

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title salt, [Ni(C7H6NO2)(C16H36N4)]ClO4 center dot H2O, the Ni-II cation is O,O'-chelated by the benzoate anion andN,N',N '',N'''-chelated by the macrocycle ligand, confering a distorted octahedral geometry on the metal atom. The complex cations, perchlorate anions and uncoordinated water molecules are linked by N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds into a three-dimensional network. The perchlorate ion is disordered over two positions in a 0.554 (8):0.446 (8) ratio.

引用

页码：M1295 / U1167

页数：14

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