Top seeded solution growth and optical properties of a bromic borate crystal: K3B6O10Br

被引：27
|
作者：
Fan, Xiaoyun [1 ,2 ]
Zhang, Min [1 ,2 ]
Pan, Shilie [1 ]
Yang, Yun [1 ,2 ]
Zhao, Wenwu [1 ,2 ]
机构：
[1] Chinese Acad Sci, Xinjiang Key Lab Elect Informat Mat & Devices, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China
[2] Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
来源：
MATERIALS LETTERS | 2012年 / 68卷
基金：
中国国家自然科学基金;
关键词：
Crystal growth; Optical materials and properties; Volatility; Borate; K3B6O10Br;
D O I：
10.1016/j.matlet.2011.11.021
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A sizable single crystal with sizes up to 20 mmx 20 mm x 9 mm of K3B6O10Br with high transparency has been grown by top seeded solution method using KF and PbO as the fluxes at the cooling rates of 0.2-0.8 degrees C/day, in the temperature range of 570-610 degrees C. Crystal morphologies and growth habits of K3B6O10Br grown using [101] and [211] direction seeds were studied. The volatility of the crystal growth systems was investigated by TG-DSC, which shows that the volatilization status is sensitive to the crystal growth temperature. The grown crystals were characterized by powder X-ray diffraction, infrared spectroscopy and transmittance spectrum. (C) 2011 Elsevier B.V. All rights reserved.
引用
收藏
页码：374 / 377
页数：4
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