Phosphorylation of per-6-O[(tert-butyl)dimethylsilyl]-β-cyclodextrin with tetraethylphosphorodiamidochloridite

被引：1

作者：

Kurochkina, GI ^{[1
]}

Kudryavtseva, NA ^{[1
]}

Soboleva, NO ^{[1
]}

Grachev, MK ^{[1
]}

Nifant'ev, EE ^{[1
]}

机构：

[1] Moscow State Pedag Univ, Moscow 119435, Russia

来源：

RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2005年 / 75卷 / 08期

基金：

俄罗斯基础研究基金会;

关键词：

Hydroxy Group; Dimethylsilyl; Primary Hydroxy Group; Hexaethylphosphorous Triamide;

D O I：

10.1007/s11176-005-0396-6

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Phosphorylation of beta-cyclodextrin with protected primary hydroxy groups with tetraethylphosphorodiamidochloridite, contrary to phosphorylation with hexaethylphosphorous triamide, proceeds irregularly and leads to compounds with mixed functions, whose ratio depends on reaction conditions.

引用

页码：1204 / 1207

页数：4

共 50 条

[11] PHOSPHORYLATION OF ALKYL TERT-BUTYL ETHERS
KOCHETKO.NK
KLIMOV, EM
KOROTEEV, MP
NIFANTEV, EE
[J]. IZVESTIYA AKADEMII NAUK SSSR-SERIYA KHIMICHESKAYA, 1972, (08): : 1867 - +
[12] Features of phosphorylation of Per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin with a phosphorous diamidoester
G. I. Kurochkina
I. A. Senyushkina
M. K. Grachev
L. K. Vasyanina
E. E. Nifant’ev
[J]. Russian Journal of General Chemistry, 2008, 78 : 61 - 64
[13] Features of phosphorylation of Per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin with a phosphorous diamidoester
Kurochkina, G. I.
Senyushkina, I. A.
Grachev, M. K.
Vasyanina, L. K.
Nifant'ev, E. E.
[J]. RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2008, 78 (01) : 61 - 64
[14] The functionalization of O-tert-butyl dimethylsilyl oximes.
Hernández-Torres, JM
Ortiz-Marciales, M
[J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 217 : U348 - U349
[15] Cyclophosphorylation of Per-6-O-(tert-butyldimethylsilyl)- β-cyclodextrin
M. K. Grachev
G. I. Kurochkina
A. A. Sutyagin
A. E. Glazyrin
E. E. Nifant'ev
[J]. Russian Journal of General Chemistry, 2001, 71 : 881 - 883
[16] Cyclophosphorylation of per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin
Grachev, MK
Kurochkina, GI
Sutyagin, AA
Glazyrin, AE
Nifant'ev, EE
[J]. RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2001, 71 (06) : 881 - 883
[17] INFLUENCE OF TERT-BUTYL ALCOHOL ON CYCLODEXTRIN INCLUSION COMPLEXES OF PYRENE
NELSON, G
PATONAY, G
WARNER, IM
[J]. JOURNAL OF INCLUSION PHENOMENA, 1988, 6 (03): : 277 - 289
[18] Phosphorylation of per-6-bromo-per-deoxy-β-cyclodextrin
Grachev, MK
Mustafin, IG
Nifantev, EE
[J]. ZHURNAL OBSHCHEI KHIMII, 1998, 68 (09): : 1519 - 1523
[19] O-METALATED STRUCTURE OF TERT-BUTYL LITHIOCYCLOALCANECARBOXYLATES
GORRICHON, L
MARONI, P
ZEDDE, C
DOBREV, A
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1983, 252 (03) : 267 - 274
[20] TERT-BUTYL DIMETHYLSILYL ETHERS AS DERIVATIVES FOR QUALITATIVE ANALYSIS OF STEROIDS AND PROSTAGLANDINS BY GAS-PHASE METHODS
KELLY, RW
TAYLOR, PL
[J]. ANALYTICAL CHEMISTRY, 1976, 48 (03) : 465 - 467

← 1 2 3 4 5 →