Phosphorylation of per-6-O[(tert-butyl)dimethylsilyl]-β-cyclodextrin with tetraethylphosphorodiamidochloridite

被引：1

作者：

Kurochkina, GI ^{[1
]}

Kudryavtseva, NA ^{[1
]}

Soboleva, NO ^{[1
]}

Grachev, MK ^{[1
]}

Nifant'ev, EE ^{[1
]}

机构：

[1] Moscow State Pedag Univ, Moscow 119435, Russia

来源：

RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2005年 / 75卷 / 08期

基金：

俄罗斯基础研究基金会;

关键词：

Hydroxy Group; Dimethylsilyl; Primary Hydroxy Group; Hexaethylphosphorous Triamide;

D O I：

10.1007/s11176-005-0396-6

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Phosphorylation of beta-cyclodextrin with protected primary hydroxy groups with tetraethylphosphorodiamidochloridite, contrary to phosphorylation with hexaethylphosphorous triamide, proceeds irregularly and leads to compounds with mixed functions, whose ratio depends on reaction conditions.

引用

页码：1204 / 1207

页数：4

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[1] Phosphorylation of Per-6-O-[(tert-butyl)dimethylsilyl]-β-cyclodextrin with Tetraethylphosphorodiamidochloridite
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[2] Phosphorylation of Per-6-O-(tert-butyl)(dimethyl)silyl-β-cyclodextrin with diethyl phosphorochloridite
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