Continuous flow time-resolved small-angle x-ray scattering and X-ray absorption spectroscopy

被引：2
|
作者：
Mo, Guang [1 ]
Wu, Zhonghua [1 ]
Cai, Quan [1 ]
Li, Zhihong [1 ]
Xing, Xueqing [1 ]
Chen, Zhongjun [1 ]
Wang, Jiayi [1 ,2 ]
Wang, Chenglong [3 ]
Liu, Guanghua [3 ]
机构：
[1] Chinese Acad Sci, Inst High Energy Phys, Beijing Synchrotron Radiat Facil, Beijing, Peoples R China
[2] Chinese Acad Sci, Grad Univ, Acad Sci, Beijing, Peoples R China
[3] Tianjin Polytech Univ, Coll Sci, Tianjin, Peoples R China
来源：
INSTRUMENTATION SCIENCE & TECHNOLOGY | 2016年 / 44卷 / 05期
基金：
中国国家自然科学基金;
关键词：
Continuous flow device; small angle x-ray scattering; x-ray absorption spectroscopy; PHASE SYNTHESIS; PETRA III; NANOPARTICLES; MICROMIXERS; BEAMLINE; KINETICS; PROTEIN; GROWTH; MIXER; CELLS;
D O I：
10.1080/10739149.2016.1153487
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A continuous flow device to characterize the growth of nanometer particles was assembled. In-situ millisecond or second-order time-resolved small angle x-ray scattering and x-ray absorption spectroscopy was performed using this device at the Beijing Synchrotron Radiation Facility. The time resolution was adjusted from 10ms to 1.0s by changing the flow rate of the solution. The temperature was variable from 5-95 degrees C. Custom-designed pulse eliminators were employed to eliminate adverse pump fluctuations and improve the quality of measurements. The system was used to characterize zinc sulfide nanoparticles by small angle x-ray scattering and x-ray absorption spectroscopy.
引用
收藏
页码：537 / 546
页数：10
相关论文
共 50 条
  • [21] Multistage Collapse of a Bacterial Ribozyme Observed by Time-Resolved Small-Angle X-ray Scattering
    Roh, Joon Ho
    Guo, Liang
    Kilburn, J. Duncan
    Briber, Robert M.
    Irving, Thomas
    Woodson, Sarah A.
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2010, 132 (29) : 10148 - 10154
  • [22] In situ tensile testing of human aortas by time-resolved small-angle X-ray scattering
    Schmid, F
    Sommer, G
    Rappolt, M
    Schulze-Bauer, CAJ
    Regitnig, P
    Holzapfel, GA
    Laggner, P
    Amenitsch, H
    JOURNAL OF SYNCHROTRON RADIATION, 2005, 12 : 727 - 733
  • [23] Time-resolved crystallization study of absorbable polymers by synchrotron small-angle X-ray scattering
    Andjelic, Sasa, 2001, John Wiley & Sons Inc, New York, NY, United States (39)
  • [24] Morphology of polyanhydride copolymers: Time-resolved small-angle X-ray scattering studies of crystallization
    Kipper, MJ
    Seifert, S
    Thiyagarajan, P
    Narasimhan, B
    JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 2005, 43 (05) : 463 - 477
  • [25] Structural Kinetics of MsbA Investigated by Stopped-Flow Time-Resolved Small-Angle X-Ray Scattering
    Josts, Inokentijs
    Gao, Yunyun
    Monteiro, Diana C. F.
    Niebling, Stephan
    Nitsche, Julius
    Veith, Katharina
    Graewert, Tobias W.
    Blanchet, Clement E.
    Schroer, Martin A.
    Huse, Nils
    Pearson, Arwen R.
    Svergun, Dmitri, I
    Tidow, Henning
    STRUCTURE, 2020, 28 (03) : 348 - +
  • [26] Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy
    Miaja-Avila, L.
    O'Neil, G. C.
    Uhlig, J.
    Cromer, C. L.
    Dowell, M. L.
    Jimenez, R.
    Hoover, A. S.
    Silverman, K. L.
    Ullom, J. N.
    STRUCTURAL DYNAMICS-US, 2015, 2 (02):
  • [27] Identifying the major intermediate species by combining time-resolved X-ray solution scattering and X-ray absorption spectroscopy
    Kim, Kyung Hwan
    Kim, Jeongho
    Oang, Key Young
    Lee, Jae Hyuk
    Grolimund, Daniel
    Milne, Christopher J.
    Penfold, Thomas J.
    Johnson, Steven L.
    Galler, Andreas
    Kim, Tae Wu
    Kim, Jong Goo
    Suh, Deokbeom
    Moon, Jiwon
    Kim, Joonghan
    Hong, Kiryong
    Guerin, Laurent
    Kim, Tae Kyu
    Wulff, Michael
    Bresslerg, Christian
    Ihee, Hyotcherl
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2015, 17 (36) : 23298 - 23302
  • [28] Virus Dynamics Studied by Time-Resolved Small Angle X-Ray Scattering
    Emeterio, Josue San
    Pollack, Lois
    BIOPHYSICAL JOURNAL, 2019, 116 (03) : 431A - 431A
  • [29] Time-resolved small-angle X-ray scattering and wide-angle X-ray diffraction studies on the nanostructure of melt-processable molecular composites
    Janicki, J
    JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 : 986 - 990
  • [30] Minireview: Structural Insights into Early Folding Events Using Continuous-Flow Time-Resolved Small-Angle X-Ray Scattering
    Kathuria, Sagar V.
    Guo, Liang
    Graceffa, Rita
    Barrea, Raul
    Nobrega, R. Paul
    Matthews, C. Robert
    Irving, Thomas C.
    Bilsel, Osman
    BIOPOLYMERS, 2011, 95 (08) : 550 - 558
12345