Synthesis and Fungicidal Activity of 1,3-Thiazoline Derivatives Bearing Nitrophenyl Group on the 2-Position

被引：2
|
作者：
Zhao, Qiuying [1 ,2 ]
Li, Jing [1 ,2 ]
Yan, Xiaojing [1 ,2 ]
Yuan, Huizhu [1 ,2 ]
Qin, Zhaohai [1 ,2 ]
Fu, Bin [1 ,2 ]
机构：
[1] China Agr Univ, Dept Appl Chem, Key Lab Pesticide Chem & Applicat Technol, Beijing 100193, Peoples R China
[2] Chinese Acad Agr Sci, Inst Plant Protect, Beijing 100193, Peoples R China
来源：
JOURNAL OF HETEROCYCLIC CHEMISTRY | 2011年 / 48卷 / 03期
关键词：
LIGANDS; THIAZOLINES; OXAZOLINES; ALKYLATION; CHEMISTRY;
D O I：
10.1002/jhet.570
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Ortho-, meta-, or para-nitro benzoic acid were refluxed with excess SOCl(2) to give acyl chloride, which condensed with beta-amino alcohol in the presence of Et(3)N in dichloromethane to afford beta-hydroxyamide; finally, sulphonation and cyclization were simultaneously conducted to afford 1,3-thiazoline derivatives. Fungicidal activity of these new thiazolines against eight agrocultural fungi were evaluated, and two of this type of compounds displayed good fungicidal activity comparable or superior to commercial fungicide chlorothalonil against two fungi at a concentration of 50 mg/L.
引用
收藏
页码：729 / 732
页数：4
相关论文
共 50 条
  • [21] Synthesis of nitrophenyl-substituted 1,3-thiazoline-2-thiones by oxirane ring opening with several dithiocarbamates
    I. V. Kulakov
    A. M. Gazaliev
    O. A. Nurkenov
    D. M. Turdybekov
    Chemistry of Heterocyclic Compounds, 2010, 46 : 490 - 494
  • [22] SYNTHESIS OF NITROPHENYL-SUBSTITUTED 1,3-THIAZOLINE-2-THIONES BY OXIRANE RING OPENING WITH SEVERAL DITHIOCARBAMATES
    Kulakov, I. V.
    Gazaliev, A. M.
    Nurkenov, O. A.
    Turdybekov, D. M.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2010, 46 (04) : 490 - 494
  • [23] Synthesis and structure of azobenzenes bearing silyl, germyl, and stannyl groups at 2-position
    Kano, N
    Komatsu, F
    Kawashima, T
    CHEMISTRY LETTERS, 2001, (04) : 338 - 339
  • [24] Syntheses of 1,3-imidazoline-2-thione and 2-phenylimino-1,3-thiazoline combinatorial libraries through different sequences of the same components
    Bae, S
    Hahn, HG
    Dal Nam, K
    JOURNAL OF COMBINATORIAL CHEMISTRY, 2005, 7 (06): : 826 - 836
  • [25] Synthesis of 1,2,4-Triazole Benzamide Derivatives and Fungicidal Activity
    Jiang, Zhenhua
    Cheng, Yi'nan
    Shen, Guofu
    Zhang, Mengmeng
    Su, Ziyang
    Sun, Liansheng
    Li, Honglian
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2020, 40 (08) : 2575 - 2582
  • [26] Synthesis and fungicidal activity of 2,2'-bipyridine derivatives
    KellyBasetti, BM
    Cundy, DJ
    Pereira, SM
    Sasse, WHF
    Savage, GP
    Simpson, GW
    BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 1995, 5 (24) : 2989 - 2992
  • [27] THE SYNTHESIS AND FUNGICIDAL ACTIVITY OF DERIVATIVES OF SORAPHEN-A SUBSTITUTED AT POSITION-12
    HOFLE, G
    OSULLIVAN, AC
    SUTTER, M
    PESTICIDE SCIENCE, 1995, 43 (04): : 358 - 361
  • [28] Synthesis and properties of bi- and tricyclic 1,3-thiazoline/thiazolidine assemblies linked by an exocyclic C=C double bond
    Obydennov, Konstantin L.
    Glukhareva, Tatiana V.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2019, 55 (11) : 1013 - 1034
  • [29] FUNGICIDAL ACTIVITY OF SOME 2-NITROPROPANEDI-1,3-OL DERIVATIVES
    ECKSTEIN, Z
    URBANSKI, T
    KOWALIK, R
    GROCHOWSKI, E
    BULLETIN DE L ACADEMIE POLONAISE DES SCIENCES-SERIE DES SCIENCES CHIMIQUES, 1963, 11 (12): : 687 - &
  • [30] Synthesis and Biological Activity of 2-Indolyl Oxazoline and Thiazoline Derivatives
    Liu, Lei
    Zheng, Zhong-Bo
    Qin, Zhao-Hai
    Fu, Bin
    Yuan, Hui-Zhu
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2008, 28 (10) : 1841 - 1845
12345