Nano-Fe3O4@SiO2 supported ionic liquid as an efficient catalyst for the synthesis of 1,3-thiazolidin-4-ones under solvent-free conditions

被引：129

作者：

Azgomi, Naghmeh ^{[1
]}

Mokhtary, Masoud ^{[1
]}

机构：

[1] Islamic Azad Univ, Rasht Branch, Dept Chem, Rasht, Iran

来源：

JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL | 2015年 / 398卷

关键词：

Fe3O4@SiO2 nanoparticles; 1,3-Thiazolidin-4-one; Ionic liquid; Solvent-free; Multicomponent reaction; ONE-POT SYNTHESIS; 4-THIAZOLIDINONES;

D O I：

10.1016/j.molcata.2014.11.018

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A magnetically supported ionic liquid on Fe3O4@SiO2 nanoparticles (MNPs@SiO2-IL) was synthesized and evaluated as a recoverable catalyst for the one-pot synthesis of 1,3-thiazolidin-4-ones in high to excellent yield under solvent-free conditions. The MNPs@SiO2-IL catalyst was characterized via Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), transmission electron microscopy (TEM) and vibrating sample magnetometer (VSM). Moreover, the catalyst could be easily recovered by magnetic separation and recycled for 10 times without significant loss of its catalytic activity. (C) 2014 Elsevier B.V. All rights reserved.

引用

页码：58 / 64

页数：7

共 50 条

[41] Synthesis of [P4-VP]-Fe3O4 supported Bronsted acid ionic liquid and its application as a highly efficient heterogeneous and reusable nanocatalyst in the Biginelli reaction under solvent-free conditions
Zarchi, Mohammad Ali Karimi
Hamidi, Zeinab
REACTION KINETICS MECHANISMS AND CATALYSIS, 2018, 125 (02) : 1023 - 1037
[42] One-pot sonochemical synthesis of 1,3-thiazolidin-4-ones using nano-CdZr4(PO4)6 as a robust heterogeneous catalyst
Safaei-Ghomi, Javad
Navvab, Maryam
Shahbazi-Alavi, Hossein
ULTRASONICS SONOCHEMISTRY, 2016, 31 : 102 - 106
[43] Magnetized inorganic-bioorganic nanohybrid [nano Fe3O4-SiO2@Glu-Cu (II)]: A novel nanostructure for the efficient solvent-free synthesis of thiazolidin-2-imines
Molaei Yielzoleh, Fatemeh
Nikoofar, Kobra
APPLIED ORGANOMETALLIC CHEMISTRY, 2021, 35 (01)
[44] Fe(OTs)3/SiO2: a novel catalyst for the multicomponent synthesis of dibenzodiazepines under solvent-free conditions
Tarannum, Saima
Siddiqui, Zeba N.
RSC ADVANCES, 2015, 5 (91): : 74242 - 74250
[45] Schiff base complex of metal ions supported on superparamagnetic Fe3O4@SiO2 nanoparticles: An efficient, selective and recyclable catalyst for synthesis of 1,1-diacetates from aldehydes under solvent-free conditions
Esmaeilpour, Mohsen
Sardarian, Ali Reza
Javidi, Jaber
APPLIED CATALYSIS A-GENERAL, 2012, 445 : 359 - 367
[46] Nano-SnCl4 • SiO2: An efficient catalyst for one-pot synthesis of 2,4,5-tri substituted imidazoles under solvent-free conditions
Mirjalili, B. F.
Bamoniri, A.
Mirhoseini, M. A.
SCIENTIA IRANICA, 2013, 20 (03) : 587 - 591
[47] Fe3O4 Nanoparticles as Highly Efficient and Recyclable Catalyst for the Synthesis of 4-Hydroxy-3-[aryloyl(benzamido)methyl] coumarin under Solvent-Free Conditions
Khodabakhshi, Saeed
Abbasabadi, Masoud Khaleghi
Heydarian, Samaneh
Shirazi, Sanaz Gharehzadeh
Marahel, Farzaneh
LETTERS IN ORGANIC CHEMISTRY, 2015, 12 (07) : 465 - 470
[48] Bronsted acidic ionic liquid as an efficient catalyst for chemoselective synthesis of 1,1-diacetates under solvent-free conditions
Hajipour, Abdol R.
Khazdooz, Leila
Ruoho, Arnold E.
CATALYSIS COMMUNICATIONS, 2008, 9 (01) : 89 - 96
[49] NaHSO4/SiO2: An Efficient Catalyst for the Synthesis of beta-Enaminones and 2-Methylquinolin-4(1H)-Ones under Solvent-Free Condition
Sapkal, Suryakant B.
Shelke, Kiran F.
Shingate, Bapurao B.
Shingare, Murlidhar S.
JOURNAL OF THE KOREAN CHEMICAL SOCIETY-DAEHAN HWAHAK HOE JEE, 2010, 54 (06): : 723 - 726
[50] Ionic Liquid Catalyzed 4,6-Disubstituted-3-Cyano-2-Pyridone Synthesis Under Solvent-Free Conditions
Sunil S. Chavan
Mariam S. Degani
Catalysis Letters, 2011, 141 : 1693 - 1697

← 1 2 3 4 5 →