Hydrothermal synthesis and characterization of a zinc-cobalt phosphate microporous material

被引：6
|
作者：
Liu, L [1 ]
Meng, H [1 ]
Li, GH [1 ]
Cui, YJ [1 ]
Ding, H [1 ]
Xing, Y [1 ]
Pang, WQ [1 ]
机构：
[1] Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China
来源：
MATERIALS LETTERS | 2005年 / 59卷 / 14-15期
基金：
中国国家自然科学基金;
关键词：
zinc-cobalt phosphate; hydrothermal synthesis; crystal structure; XRD; magnetic materials;
D O I：
10.1016/j.matlet.2005.01.059
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A new zinc-cobalt phosphate compound [Zn(4-x)COx(PO4)(2)(HPO4)][C3H4N2](3) (x=0.25) (1) has been hydrothermally synthesized in the presence of imidazole as the template and crystallizes in the triclinic space group P-1 with crystal data a=9.6077(7) angstrom, b=9.8674(7) angstrom, c=12.3793(9) angstrom, alpha=77.569(4)degrees, beta=78.040(4)degrees, gamma=68.191(4)degrees, V=1053.52(13) angstrom(3), Z=2. Compound 1 exhibits an infinite two-dimensional layered structure, which is built up Of {M8P6O23} structural unit formed by vertex-sharing MO4, MO2N2, MO3N, PO4 and PO3(OH) (M=Zn, Co) moieties. A study of magnetic measurements indicates compound I has the well antiferromagnetic behavior. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码：1752 / 1755
页数：4
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