A simple, rapid and efficient protocol for the selective phosphorylation of phenols with dibenzyl phosphite

被引:74
|
作者
Silverberg, LJ
Dillon, JL
Vemishetti, P
机构
[1] Bristol-Myers Squibb Company, Process Exploration Labs., Syracuse, NY 13221-4755
关键词
D O I
10.1016/0040-4039(95)02294-5
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Phosphorylation of phenols with dibenzyl phosphite, carbon tetrachloride, N,N-diisopropylethylamine, and catalytic DMAP in acetonitrile at -10 degrees C is rapid, mild, clean, high yielding, and selective.
引用
收藏
页码:771 / 774
页数:4
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