Syntheses and characterization of two metal-organic frameworks with in situ-generated 5-(4-pyridyl)tetrazolate and azide

被引：13

作者：

Yang, Yu-Ting ^{[1
]}

Zhao, Fang-Hua ^{[1
]}

Che, Yun-Xia ^{[1
]}

Zheng, Ji-Min ^{[1
]}

机构：

[1] Nankai Univ, Dept Chem, Tianjin 300071, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2011年 / 14卷 / 12期

基金：

中国国家自然科学基金;

关键词：

Hydro(solvo)thermal synthesis; In situ; Azide; (3,5,6)-connected; Luminescence; COORDINATION POLYMERS; 5-SUBSTITUTED; 1H-TETRAZOLES; ADSORPTION; COMPLEXES; ROUTE;

D O I：

10.1016/j.inoche.2011.08.011

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two novel metal-organic frameworks of [M-3(ptz)(2)(N-3)(4)(H2O)(2)] (M = Zn(1), Cd(2)) (Ptz = 5-(4-pyridyl)tetrazolate) have been prepared hydro(solvo)thermally by reactions of 4-cyanopyridine and excess NaN3 in the presence of zinc and cadmium chloride, respectively. The overall structure motif of complexes 1 and 2 show pillared layered frameworks and feature an unprecedented 3-nodal network with (3,5,6)-connectivity. The layer is of particular interest as it is constructed by mu(1,1)-N-3(-) and mu(1,1,3)-N-3(-) bridging modes, simultaneously. Furthermore, the solid fluorescent properties and TGA were studied. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：1855 / 1859

页数：5

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