Synthesis of cholic acid amino analogues by oxime reduction with TiCl3-NaBH3CN

被引：3
|
作者：
Maslov, Mikhail A. [1 ]
Morozova, Nina G. [1 ]
Solomatina, Tatyana V. [1 ]
Sergeeva, Olga A. [1 ]
Cheshkov, Dmitry A. [2 ]
Serebrennikova, Galina A. [1 ]
机构：
[1] MV Lomonosov Moscow State Acad Fine Chem Technol, Moscow 119571, Russia
[2] State Res Inst Chem & Technol Organoelement Cpds, Moscow 111123, Russia
来源：
MENDELEEV COMMUNICATIONS | 2011年 / 21卷 / 03期
基金：
俄罗斯基础研究基金会;
关键词：
UMBRELLA-ASSISTED TRANSPORT; TRIAMINO-ANALOG; FACIAL AMPHIPHILES; METHYL CHOLATE; DRUG-DELIVERY; RECEPTORS; DERIVATIVES; SELECTIVITY; OXIDATION;
D O I：
10.1016/j.mencom.2011.04.007
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Amino analogues of cholic acid have been synthesized by reduction of the corresponding oximes with titanium(III) chloride in the presence of sodium cyanoborohydride.
引用
收藏
页码：137 / 139
页数：3
相关论文
共 50 条
  • [31] Cu(I)-Catalyzed Synthesis of Dihydropyrimidin-4-ones toward the Preparation of β- and β3-Amino Acid Analogues
    Rajagopal, Basker
    Chen, Ying-Yu
    Chen, Chun-Chi
    Liu, Xuan-Yu
    Wang, Huei-Ren
    Lin, Po-Chiao
    JOURNAL OF ORGANIC CHEMISTRY, 2014, 79 (03): : 1254 - 1264
  • [32] Synthesis and anti-CVB3 activity of 4-amino acid derivative substituted pyrimidine nucleoside analogues
    Tao, Le
    Li, Yujiang
    Guo, Xiaohe
    Dong, Lihong
    Liu, Luping
    Wang, Qiang
    Yu, Xuejun
    Song, Chuanjun
    Chang, Junbiao
    BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2020, 30 (01)
  • [33] FORMATION OF BIS (FMOC-AMINO ETHYL)-N-GLYCINE DERIVATIVES BY REDUCTIVE AMINATION OF FMOC-AMINO ALDEHYDES WITH NABH3CN
    SALVI, JP
    WALCHSHOFER, N
    PARIS, J
    TETRAHEDRON LETTERS, 1994, 35 (08) : 1181 - 1184
  • [34] Synthesis of amino acid derivatives of indole-3-acetic acid
    Liu, Y
    Zhao, L
    Liu, L
    Wei, LY
    Lai, LH
    JOURNAL OF CHEMICAL RESEARCH, 2005, (10) : 640 - 642
  • [35] Synthesis of 3-amino-5-nitrobenzaldehyde oxime and its conversion into 3,4-bis(3-amino-5-nitrophenyl)furoxan and isomeric 3(4)-(3-amino-5-nitrophenyl)-4(3)-nitrofuroxans
    M. A. Epishina
    I. V. Ovchinnikov
    N. N. Makhova
    Russian Chemical Bulletin, 1997, 46 : 2117 - 2120
  • [36] Synthesis and Biological Activities of 3-Substituted Analogues of Tenuazonic Acid
    Liu, Yu-Xiu
    Cui, Zhi-Peng
    Zhao, Hua-Ping
    Li, Yong-Hong
    Gu, Yu-Cheng
    Wang, Qing-Min
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2014, 51 : E209 - E215
  • [37] Synthesis of 3-amino-5-nitrobenzaldehyde oxime and its conversion into 3,4-bis(3-amino-5-nitrophenyl)furoxan and isomeric 3(4)-(3-amino-5-nitrophenyl)-4(3)-nitrofuroxans
    Epishina, MA
    Ovchinnikov, IV
    Makhova, NN
    RUSSIAN CHEMICAL BULLETIN, 1997, 46 (12) : 2117 - 2120
  • [38] SYNTHESIS OF AMINO-ACIDS BY ELECTROCHEMICAL REDUCTION .3. SYNTHESIS OF SERINE BY ELECTROCHEMICAL REDUCTION OF (HYDROXYIMINO) MALONAMIC ACID METHYL-ESTER
    KOKUSENYA, Y
    NAKAJIMA, S
    MATSUOKA, M
    DENKI KAGAKU, 1987, 55 (03): : 235 - 238
  • [39] 3-Pyrazolone analogues of the 3-isoxazolol metabotropic excitatory amino acid receptor agonist homo-AMPA.: Synthesis and pharmacological testing
    Zimmermann, D
    Janin, YL
    Brehm, L
    Bräuner-Osborne, H
    Ebert, B
    Johansen, TN
    Madsen, U
    Krogsgaard-Larsen, P
    EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 1999, 34 (11) : 967 - 976
  • [40] Convergent synthesis and pharmacology of substituted tetrazolyl-2-amino-3-(3-hydroxy-5-methyl-4-isoxazolyl)propionic acid analogues
    Vogensen, SB
    Clausen, RP
    Greenwood, JR
    Johansen, TN
    Pickering, DS
    Nielsen, B
    Ebert, B
    Krogsgaard-Larsen, P
    JOURNAL OF MEDICINAL CHEMISTRY, 2005, 48 (09) : 3438 - 3442
12345