Non-enzymatic hydrogen peroxide sensor using an electrode modified with iron pentacyanonitrosylferrate nanoparticles

被引：25
|
作者：
Razmi, Habib [1 ]
Mohammad-Rezaei, Rahim [1 ]
机构：
[1] Azarbaijan Univ Tarbiat Moallem, Electrochem Res Lab, Fac Sci, Tabriz, Iran
来源：
MICROCHIMICA ACTA | 2010年 / 171卷 / 3-4期
关键词：
Hydrogen peroxide; Iron pentacyanonitrosylferrate; Modified electrode; Electrocatalysis; GLASSY-CARBON ELECTRODE; QUARTZ-CRYSTAL MICROBALANCE; PRUSSIAN-BLUE; INDIUM HEXACYANOFERRATE; COBALT HEXACYANOFERRATE; HORSERADISH-PEROXIDASE; CERAMIC ELECTRODE; REDOX REACTIONS; FILM GROWTH; OXIDATION;
D O I：
10.1007/s00604-010-0426-x
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
An electrochemical sensor was developed for determination of hydrogen peroxide (HP) based on a carbon ceramic electrode modified with iron pentacyanonitrosyl-ferrate (FePCNF). The surface of an iron-doped CCE was derivatized in a solution of PCNF by cycling the electrode potential between -0.2 and +1.3 V for about 60 times. The morphology and the composition of the resulting electrode were characterized by scanning electron microscopy and Fourier transform infrared techniques. The electrode displayed excellent response to the electro-oxidation of HP which is linearly related to its concentration in the range from 0.5 mu M to 1300 mu M. The detection limit is 0.4 mu M, and the sensitivity is 849 A M (-1)cm (-2). The modified electrode was used to determination of HP in hair coloring creams as real samples.
引用
收藏
页码：257 / 265
页数：9
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