Hydrothermal synthesis of aluminum-doped zincophosphate large single crystal with different morphology

被引：3

作者：

Shi, W. T. ^{[1
]}

Sun, D. L. ^{[1
]}

Chen, J. Q. ^{[1
]}

Sun, L. ^{[1
]}

Chu, S. W. ^{[1
]}

Xi, Z. ^{[2
]}

Zeng, Yu-Jia ^{[1
]}

Xu, X. T. ^{[1
]}

Ruan, S. C. ^{[1
]}

机构：

[1] Shenzhen Univ, Shenzhen Key Lab Laser Engn, Shenzhen 518060, Peoples R China

[2] Shenzhen Univ, Electron Microscopy Ctr, Shenzhen 518060, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2019年 / 507卷

基金：

中国国家自然科学基金; 中国博士后科学基金;

关键词：

Crystal morphology; Hydrothermal crystal growth; Single crystal growth; Phosphates; ALUMINOPHOSPHATE MOLECULAR-SIEVE; PHOSPHATE; SILICA; ZINC; GROWTH; ROUTE;

D O I：

10.1016/j.jcrysgro.2018.11.004

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Large single crystals of Aluminum-zincohposphate (AlZnPO4-DFT) with different morphology have been hydrothermally synthesized by using ethylenediamine (EDA) as structure-directing agent. The effects of crystallization conditions and gel compositions on products were investigated in detail. The pure phase with DFT structure could be obtained at 170 degrees C, while the competitive phase would appear when the crystallization temperature rises to 190 degrees C. The quality of AlZnPO4-DFT crystals enhances firstly and then deteriorates with the extension of crystallization duration from 20 h to 50 h. Moreover, the gel composition not only affects the size of the product, but also affects the morphology and quality of the product.

引用

页码：189 / 195

页数：7

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