A novel catalyst-free mechanochemical protocol for the synthesis of 2,3-dihydro-1H-perimidines

被引：19

作者：

Harry, Nissy Ann ^{[1
]}

Radhika, Sankaran ^{[1
]}

Neetha, Mohan ^{[1
]}

Anilkumar, Gopinathan ^{[1
,2
]}

机构：

[1] Mahatma Gandhi Univ, Sch Chem Sci, Priyadarsini Hills, Kottayam 686560, Kerala, India

[2] Mahatma Gandhi Univ, AMMRC, Kottayam, Kerala, India

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2020年 / 57卷 / 04期

关键词：

aldehyde; grinding; ketone; mechanochemistry; perimidine; EFFICIENT CATALYST; PERIMIDINE DERIVATIVES; ZEOLITE;

D O I：

10.1002/jhet.3880

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A rapid, efficient, and green grinding assisted method for the synthesis of 2,3-dihydro-1H-perimidines has been developed. 1,8-Diaminonaphthalene and aldehydes were ground using mortar and pestle for 5 minutes affording the product in moderate to excellent yields. The methodology minimises the use of conventional workup and column chromatographic techniques.

引用

页码：2037 / 2043

页数：7

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