Synthesis of Macrolides with Hydrazide Fragments from Tetrahydropyran and 2,6-Pyridinedicarboxylic Acid

被引：5

作者：

Ishmuratov, Gumer Yu. ^{[1
]}

Yakovleva, Marina P. ^{[1
]}

Shutova, Mariya A. ^{[1
]}

Yaubasarov, Niyaz R. ^{[1
]}

Muslukhov, Rinat R. ^{[1
]}

Viripaev, Evgeny M. ^{[1
]}

Tolstikov, Alexander G. ^{[1
]}

机构：

[1] RAS, Ufa Sci Ctr, Inst Organ Chem, Ufa 450054, Russia

来源：

MACROHETEROCYCLES | 2014年 / 7卷 / 03期

关键词：

Tetrahydropyran; macrolides with dihydrazide fragments; 1+1]-condensation; synthesis; DERIVATIVES; ESTER;

D O I：

10.6060/mhc140374y

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The synthesis of two potentially useful 23- and 29-membered macrolides containing a pyridine ring and dihydrazide fragments was developed starting from tetrahydropyran. It was based on [1+1]-condensation of 7'-oxooctyl-7-oxooctanoate and bis(7-oxooctyl) hexanedioate with 2,6-pyridinedicarboxylic acid hydrazide. The structure of the macrocycles obtained was confirmed using by IR and NMR spectroscopy and mass spectrometry.

引用

页码：721 / 724

页数：4

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