Synthesis, Structure, and Characterization of an Organic Compound Based on 3-Nitrobenzoic Acid Moiety

被引：4
|
作者：
Feng, Xun [1 ]
Wang, Wei-Zhou [1 ]
Li, Tie-Fu [1 ]
Shang, Jing Jing [1 ]
Wang, Li-Ya [1 ]
机构：
[1] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang 471022, Peoples R China
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2012年 / 42卷 / 01期
基金：
中国国家自然科学基金;
关键词：
density functional theory calculations; dithio compound; luminescent property; X-ray single structure; COORDINATION POLYMERS; CRYSTAL-STRUCTURE; DISULFIDE; COMPLEXES;
D O I：
10.1080/15533174.2011.609222
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
An organic compound 5,5'dithio-bis-2-nitrobenzoic formate, formulated as C16H12N2O8S2 (1) has been synthesized and characterized by elemental analysis, IR, UV, transmission Raman spectroscopy, and X-ray single crystal diffraction. It crystallizes in a monoclinic system, space group P-1, with a = 8.041(2), b = 10.036(3), c = 11.340(3) angstrom, V = 876.8 angstrom(3). The pi-pi stacking interactions propagate the compound unit into a trimer structure, and these trimers are further linked by intermolecular pi-pi stacking interactions into the two-dimensional supramolecular network. Compound 1 displays strong photoluminescent properties in the liquid state, as well as the obvious Raman shift.
引用
收藏
页码：18 / 24
页数：7
相关论文
共 50 条
  • [21] Experimental and computational chemistry studies on the inhibition of aluminium and mild steel in 0.1 M HCl by 3-nitrobenzoic acid
    Eddy, Nnabuk Okon
    Ameh, Paul Ocheje
    Essien, Nsikak Bassey
    JOURNAL OF TAIBAH UNIVERSITY FOR SCIENCE, 2018, 12 (05): : 545 - 556
  • [22] Electrochemical evidence of nitrate release from the nitrooxy compound 4-((nitrooxy) methyl)-3-nitrobenzoic acid and its antinociceptive and anti-inflammatory activities in mice
    Braga, Alysson Vinicius
    Lisboa da Silva, Roger Ryuler
    Rodrigues, Ianny Bandeira
    de Lima Marques, Gabriel Vitor
    de Almeida Xavier, Andre Felippe
    Boane, Anastacio
    Branda de Paiva, Mayara Rodrigues
    Cavalcanti Franco, Pedro Henrique
    Rodrigues, Felipe Fernandes
    Ferraz Melo, Ivo Souza
    Cunha Junior, Armando da Silva
    Cesar, Isabela da Costa
    Fonseca Goulart, Marilia Oliveira
    de Oliveira, Renata Barbosa
    Coelho, Marcio de Matos
    Machado, Renes Resende
    BIOMEDICINE & PHARMACOTHERAPY, 2021, 133
  • [23] CHARACTERIZATION OF A NEW SULFHYDRYL-GROUP REAGENT - 6,6'-DISELENOBIS-(3-NITROBENZOIC ACID), A SELENIUM ANALOG OF ELLMAN REAGENT
    LUTHRA, NP
    DUNLAP, RB
    ODOM, JD
    ANALYTICAL BIOCHEMISTRY, 1981, 117 (01) : 94 - 102
  • [24] TRANSFER AND EXCHANGE EFFECTS IN DISSOCIATION OF 3-NITROBENZOIC ACID IN H-20 AND D-20 AND IN THEIR DMSO MIXTURES
    VESALA, A
    SALOMA, E
    ACTA CHEMICA SCANDINAVICA SERIES A-PHYSICAL AND INORGANIC CHEMISTRY, 1976, 30 (01): : 76 - 78
  • [25] DIFFERENTIAL-PULSE POLAROGRAPHIC-DETERMINATION OF NITRATE AS 3-NITROBENZOIC ACID AND OTHER NITRO-DERIVATIVES
    FOGG, AG
    SCULLION, SP
    EDMONDS, TE
    ANALYST, 1988, 113 (06) : 979 - 981
  • [26] Syntheses, structures and properties of three chiral metal-organic coordination polymers based on (R)-4-(4-(1-carboxyethoxy)phenoxy)-3-nitrobenzoic acid
    Hao, Peng
    Huang, Qi
    Gu, Lei
    Yu, Ying-Hui
    Ma, Dong-Sheng
    POLYHEDRON, 2018, 149 : 117 - 125
  • [27] A luminescent barium-based metal-organic framework: Synthesis, structure and efficient detection of 4-nitrobenzoic acid
    Xin, Xue-Huan
    Lu, Wen
    Lu, Jian
    Xu, Jian-Gang
    Wang, Shuai-Hua
    Zheng, Fa-Kun
    Guo, Guo-Cong
    INORGANIC CHEMISTRY COMMUNICATIONS, 2018, 97 : 129 - 133
  • [28] Application of polymer-bound 4-(bromomethyl)-3-nitrobenzoic acid for synthesis of trisubstituted 1,4-benzodiazepine-2,3-diones
    Jinfang Zhang
    Boliang Lou
    Hossain Saneii
    Molecular Diversity, 2003, 6 : 13 - 17
  • [29] Rapid evaluation of the substrate specificity of 3-nitrobenzoic acid dioxygenase MnbAB via colorimetric detection using Saltzman reagent
    Tomita, Hiroya
    Katsuyama, Yohei
    Ohnishi, Yasuo
    JOURNAL OF INDUSTRIAL MICROBIOLOGY & BIOTECHNOLOGY, 2021, 48 (9-10)
  • [30] SYNTHESIS OF 5-BROMOACETYL-3-NITROBENZOIC ACID
    KRASNOV, IB
    JOURNAL OF GENERAL CHEMISTRY USSR, 1962, 32 (01): : 287 - &
12345