Synthesis, Structure, and Characterization of an Organic Compound Based on 3-Nitrobenzoic Acid Moiety

被引：4

作者：

Feng, Xun ^{[1
]}

Wang, Wei-Zhou ^{[1
]}

Li, Tie-Fu ^{[1
]}

Shang, Jing Jing ^{[1
]}

Wang, Li-Ya ^{[1
]}

机构：

[1] Luoyang Normal Univ, Coll Chem & Chem Engn, Luoyang 471022, Peoples R China

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2012年 / 42卷 / 01期

基金：

中国国家自然科学基金;

关键词：

density functional theory calculations; dithio compound; luminescent property; X-ray single structure; COORDINATION POLYMERS; CRYSTAL-STRUCTURE; DISULFIDE; COMPLEXES;

D O I：

10.1080/15533174.2011.609222

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

An organic compound 5,5'dithio-bis-2-nitrobenzoic formate, formulated as C16H12N2O8S2 (1) has been synthesized and characterized by elemental analysis, IR, UV, transmission Raman spectroscopy, and X-ray single crystal diffraction. It crystallizes in a monoclinic system, space group P-1, with a = 8.041(2), b = 10.036(3), c = 11.340(3) angstrom, V = 876.8 angstrom(3). The pi-pi stacking interactions propagate the compound unit into a trimer structure, and these trimers are further linked by intermolecular pi-pi stacking interactions into the two-dimensional supramolecular network. Compound 1 displays strong photoluminescent properties in the liquid state, as well as the obvious Raman shift.

引用

页码：18 / 24

页数：7

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