Determination of volatile compounds in whiting (Merlangius merlangus) using headspace-solid-phase microextraction-gas chromatography-mass spectrometry

被引：17
|
作者：
Duflos, G [1 ]
Moine, F [1 ]
Coin, VM [1 ]
Malle, P [1 ]
机构：
[1] Agence Francaise Secur Sanitaire Aliments, Lab Etude & Rech Produits Peche, F-62200 Boulogne, France
来源：
JOURNAL OF CHROMATOGRAPHIC SCIENCE | 2005年 / 43卷 / 06期
关键词：
D O I：
10.1093/chromsci/43.6.304
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A method using headspace-solid-phase microextraction-gas chromatography-mass spectrometry to extract volatile compounds from whiting is developed. Several parameters such as sorption time, desorption time, fiber type, and matrix form are optimized to achieve better sensitivity in minimal analysis time. The efficiency of the method is determined by the linear range and repeatability; a mean relative standard deviation of approximately 7% is measured. It was possible to identify and quantitate 30 volatile compounds of interest present in spoiled whiting.
引用
收藏
页码：304 / 312
页数：9
相关论文
共 50 条
  • [1] Determination of Volatile Flavor Compounds of Shrimp Head by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Xie Wan-Cui
    Yang Xi-Hong
    Zhang Chao-Hua
    Ji Hong-Wu
    Zhang Li-Feng
    [J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2011, 39 (12) : 1852 - 1857
  • [2] Headspace solid-phase microextraction-gas chromatography-mass spectrometry characterization of propolis volatile compounds
    Pellati, Federica
    Prencipe, Francesco Pio
    Benvenuti, Stefania
    [J]. JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2013, 84 : 103 - 111
  • [3] Determination of Volatile Organic Compounds in Andean Tomato Landraces by Headspace Solid Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Cortina, Pablo R.
    Asis, Ramon
    Peralta, Iris E.
    Asprelli, Pablo D.
    Santiago, Ana N.
    [J]. JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2017, 28 (01) : 30 - 41
  • [4] Determination of butyltin compounds in seawater by headspace-solid-phase microextraction-gas chromatography
    Zhu Z.
    Jiao J.
    Chai X.
    Shi T.
    [J]. Tongji Daxue Xuebao/Journal of Tongji University, 2010, 38 (09): : 1324 - 1328
  • [5] Determination of odorous compounds in water by headspace solid-phase microextraction-gas chromatography-mass spectrometry
    Li, L
    Song, LR
    Gan, NQ
    Chen, W
    [J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2005, 33 (08) : 1058 - 1062
  • [6] Analysis of Volatile Compounds in Agaricus Bisporus by Headspace Solid-Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Yu, Xia
    Liang, Hai-Yang
    Zhao, Yan-Bo
    Cui, Li-Li
    [J]. CURRENT TOPICS IN NUTRACEUTICAL RESEARCH, 2023, 21 (04) : 524 - 530
  • [7] Analysis of Volatile Components in Rosa roxburghii Tratt. and Rosa sterilis Using Headspace-Solid-Phase Microextraction-Gas Chromatography-Mass Spectrometry
    Deng, Yuhang
    Kan, Huan
    Li, Yonghe
    Liu, Yun
    Qiu, Xu
    [J]. MOLECULES, 2023, 28 (23):
  • [8] Quantitative analysis of volatiles in transesterified coconut oil by headspace-solid-phase microextraction-gas chromatography-mass spectrometry
    Sun, Jingcan
    Yu, Bin
    Curran, Philip
    Liu, Shao-Quan
    [J]. FOOD CHEMISTRY, 2011, 129 (04) : 1882 - 1888
  • [9] Comparison of the volatile compounds of Atractylodes medicinal plants by headspace solid-phase microextraction-gas chromatography-mass spectrometry
    Guo, Fang-Qiu
    Huang, Lan-Fang
    Zhou, Shao-Yun
    Zhang, Tai-Ming
    Liang, Yi-Zeng
    [J]. ANALYTICA CHIMICA ACTA, 2006, 570 (01) : 73 - 78
  • [10] Headspace solid-phase microextraction-gas chromatography-mass spectrometry analysis of the volatile compounds of Evodia species fruits
    Pellati, F
    Benvenuti, S
    Yoshizaki, F
    Bertelli, D
    Rossi, MC
    [J]. JOURNAL OF CHROMATOGRAPHY A, 2005, 1087 (1-2) : 265 - 273
12345