Fabrication and characteristic of delafossite-type CuFeO2 nanofibers by electrospinning method

被引:8
|
作者
Chao, Tzu-Chia [1 ]
Chiu, Te-Wei [1 ]
Fu, Yongsheng [2 ]
机构
[1] Natl Taipei Univ Technol, Dept Mat & Mineral Resources Engn, 1,Sect 3,Zhongxiao E Rd, Taipei 106, Taiwan
[2] Nanjing Univ Sci & Technol, Key Lab Soft Chem & Funct Mat, Nanjing 210094, Jiangsu, Peoples R China
关键词
Delafossite structure; Electrospinning; CuFeO2; Nanofibers; Optical properties; THIN-FILMS;
D O I
10.1016/j.ceramint.2018.08.235
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
CuFeO2 delafossite type nano fibers were fabricated by electrospinning. This experiment explored the effects of annealing temperature, precursor concentration, and ambient annealing on the fiber structure. The results of X-ray diffraction studies (XRD) and field emission scanning electronic microscopy (FESEM) indicated that a pure phase delafossite-type CuFeO2 and perfect nanofibers can be synthesized by annealing at 500 degrees C in air for 10 min and 750 degrees C in nitrogen for 10 min. The optical properties were measured by UV/VIS spectrometer and the band gap was estimated at 1.4 eV. Furthermore, the specific surface area of the CuFeO2 fibers was 4.33 m(2)/g, as determined by BET surface area measurements.
引用
收藏
页码:S80 / S83
页数:4
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