N2,N2′-Bis[4-(dimethylamino)benzylidene]pyridine-2,6-dicarbohydrazide monohydrate

被引:0
|
作者
Wang, Yong [1 ]
Sun, Yan Liang [1 ]
机构
[1] Liaocheng Univ, Dept Chem, Liaocheng 252059, Peoples R China
关键词
D O I
10.1107/S1600536810038778
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C25H27N7O2 center dot H2O, the bis[4-(dimethylamino) benzylidene]pyridine- 2,6-dicarbohydrazide molecule and the water molecule are located on a twofold rotation axis. The benzene and pyridine rings form a dihedral angle of 17.13 (7)degrees. In the crystal, intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds link the molecules into a two-dimensional supermolecular structure parallel to the ab plane.
引用
收藏
页码:O2718 / U1732
页数:8
相关论文
共 50 条
  • [41] Tetrabutylammonium bis[N,N′-bis(4-chloro-phenyl)pyridine-2,6-dicarboxamide(1-)]-cobaltate(III) monohydrate
    Qi, Jian Ying
    Yang, Qi Yun
    Zhou, Zhong Yuan
    Chan, Albert S. C.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M159 - M161
  • [42] N,N′-Bis(4-methyl-2-benzothiazolyl)pyridine-2,6-dicarboxamide N, N-dimethylformamide solvate
    Liu, Sheng-Gui
    Ni, Chun-Lin
    Li, Yi-Zhi
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O1704 - O1705
  • [43] catena-poly[[[μ-di-4-pyridyldiazene-κ2N4:N4′-bis[(triphenylphosphine-κP)copper(I)]]-μ-pyridine-2-carbaldehyde azine-κN2,N:N′,N2′] bis(tetrafluoroborate)]
    Yu, MM
    Fu, WF
    Li, ZX
    Yao, ZF
    Jia, LF
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : M1897 - M1899
  • [44] N,N '-Bis(4-hydroxyphenyl) pyridine-2,6-dicarboxamidedimethylformamide monosolvate
    Waris, Ghulam
    Siddiqi, Humaira Masood
    Florke, Ulrich
    Hussain, Rizwan
    Butt, M. Saeed
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O991 - +
  • [45] N,N'-Bis[4-(dimethylamino)benzylidene]butane-1,4-diamine
    Habibi, Mohammad Hossein
    Zendehdel, Mahmoud
    Chantrapromma, Suchada
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4330 - U3499
  • [46] N,N′-Bis[2-(2-pyridyl)methyl]pyridine-2,6-dicarboxamide hemihydrate
    Qi, JY
    Chen, J
    Yang, QY
    Zhou, ZY
    Chan, ASC
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 : O1232 - O1233
  • [47] N′-[4-(Dimethylamino)benzylidene]-3-hydroxy-2-naphthohydrazide
    Huang, Hai-Tao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : I892 - U3166
  • [48] Rare examples of base pairing via a protonated pyridine N atom in two salts of N2,N6-bis(1,3-dimethyl-imidazolin2-ylidene)pyridine-2,6-diamine
    Neuba, Adam
    Akin, Enver
    Herres-Pawlis, Sonja
    Floerke, Ulrich
    Henkel, Gerald
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2008, 64 : M194 - M197
  • [49] N2,N2′-Bis(2-hydroxy-3-methoxybenzylidene)terephthalohydrazide dihydrate
    Qiao, Yanling
    Yin, Handong
    Cui, Jichun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4819 - U6082
  • [50] N2′,N5′-Diisopropylidenepyrazine-2,5-dicarbohydrazide dihydrate
    Ding, Miao
    Wu, Wen-Shi
    Li, Hai-Ping
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O677 - U1044