5′-(2-chlorophenyl)-1′-methyl-2",3"-dihydroindoline-3-spiro-3′-pyrrolidine-4′-spiro-2"-(1,3-benzimidazo[2,1-b]-thiazole)-2,3"-dione dioxane hemisolvate

被引：3
|
作者：
Li, XF [1 ]
Feng, YQ [1 ]
Li, G [1 ]
Wang, G [1 ]
机构：
[1] Tianjin Univ, Sch Chem Engn & Technol, State Key Lab C1 Chem Technol, Tianjin 300072, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷
关键词：
D O I：
10.1107/S1600536803017471
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C26H19ClN4O2S.0.5C(4)H(8)O(2), was synthesized by the intermolecular [3+2]-cycloaddition of azomethine ylide, derived from isatin and sarcosine by a decarboxylative route, and 2-(2-chlorobenzylidene) benzo[ 4,5] imidazo[2,1-b] thiazol-3-one. In the molecule, the two spiro junctions link a planar 2-oxoindoline ring, a pyrrolidine ring in an envelope conformation, and a planar benzo[ 4,5]imidazo[ 2,1-b] thiazol-3(2H)-one ring. Two molecules are connected by N-H...O hydrogen bonds to a molecule of dioxane on an inversion center, with an N...O distance of 2.823 (2) Angstrom.
引用
收藏
页码：O1307 / O1308
页数：2
相关论文
共 50 条
  • [1] 4′-(2,4-dichlorophenyl)-1′-methyl-2,3,2",3"-tetrahydro-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2"-(1,3-benzimidazo[2,1-b]thiazole)-2,3"-dione
    Li, XF
    Feng, YQ
    Shi, DX
    Chen, HL
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1405 - O1406
  • [2] 1′-methyl-5′-phenyl-2",3",5",6"-tetra-hydroindoline-3-spiro-3′-pyrrolidine-4′-spiro-2"-imidazo[2,1-b]thiazole-2,3"-dione
    Li, XF
    Feng, YQ
    Shi, DX
    Li, G
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O1288 - O1289
  • [3] 4′-(3-chlorophenyl)-1-methyl-1H-indole-3-spiro-2′-pyrrolidine-3′-spiro-2"-indan-2,1",3"-trione
    Seshadri, PR
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Sureshbabu, AR
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O51 - O53
  • [4] 1′-methylacenapthylene-1(2H)-spiro-2′-pyrrolidine-3′-spiro-2"(3"H)-carbazole-2,1"(4"H)-dione
    Kumar, B. K. Satis
    Gayathri, D.
    Velmurugan, D.
    Ravikumar, K.
    Periyasami, G.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O843 - O845
  • [5] 4′-(4-Chlorophenyl)-1′-methylcycloheptane-1-spiro-3′-pyrrolidine-2′-spiro-2"-indan-2,1",3"-trione
    Mamta, B.
    Gayathri, D.
    Velmurugan, D.
    Ravikumar, K.
    Poornachandran, M.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2230 - O2232
  • [6] 1′-methyl-2"-phenylcyclohexane-1-spiro-4′-[acenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-4"(5"H)-[1,3]oxazole]-2,5"-dione
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Jayashankaran, J
    Durga, RR
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O2216 - O2218
  • [7] Synthesis of spiro[imidazo[2,1-b][1,3]thiazole-6,3'-pyrrolidine] derivatives
    Lesya M. Saliyeva
    Nataliia Yu. Slyvka
    Dmitro A. Mel’nyk
    Eduard B. Rusanov
    Ruslan I. Vas’kevich
    Mikhailo V. Vovk
    Chemistry of Heterocyclic Compounds, 2018, 54 : 130 - 137
  • [8] Synthesis of spiro[imidazo[2,1-b][1,3]thiazole-6,3'-pyrrolidine] derivatives
    Saliyeva, Lesya M.
    Slyvka, Nataliia Yu
    Mel'nyk, Dmitro A.
    Rusanov, Eduard B.
    Vas'kevich, Ruslan I.
    Vovk, Mikhailo V.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2018, 54 (02) : 130 - 137
  • [9] 1′-methyl-4′-phenylacenaphthene-1-spiro-2′-pyrrolidine-3′-spiro-2"-indan-2,1"3",-trione
    Govind, MM
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Sureshbabu, AR
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2004, 60 : O547 - O549
  • [10] 3′-(2-chlorophenyl)-1′-methyl-4′-nitro-spiro[indan-2,2′-pyrrolidine]-1,3-dione
    Selvanayagam, S
    Velmurugan, D
    Ravikumar, K
    Rao, SN
    Poornachandran, M
    Raghunathan, R
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O2157 - O2159
12345