Hydrothermal syntheses, structures and characterizations of three one-dimensional polyoxomolybdates with 4,4′-dimethylenebiphenyl diphosphonic acid as bridge

被引：9
|
作者：
Zhang, HS [1 ]
Fu, RB [1 ]
Zhang, HJ [1 ]
Wu, XT [1 ]
Li, YM [1 ]
Wang, LS [1 ]
Huang, XH [1 ]
机构：
[1] Chinese Acad Sci, Fujian Inst Res Struct Matter, State Key Lab Struct Chem, Fuzhou 350002, Fujian, Peoples R China
来源：
JOURNAL OF SOLID STATE CHEMISTRY | 2005年 / 178卷 / 05期
基金：
中国国家自然科学基金;
关键词：
hydrothermal synthesis; crystal structure; metal-organic subunit; one-dimensional; polyoxomolybdate; 4,4 '-dirnethylenebiphenyldiphosphonic acid;
D O I：
10.1016/j.jssc.2005.02.013
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Three heterometallic 1-D polymers, [{Ni(1,10-phen)(2)(H2O)}(2) {(Mo5O15)(4,4'-dbp)} (.) (5.75H(2)O)] (4,4-dbp = O3PCH2C6H4C6 H4CH2PO3) (1), [{Co(1,10-phen)(2)(H2O)}(2) {(Mo5O15)(4,4'-dbp)} (.) (5.5H(2)O)] (2) and [{Ni(2,2'-bpy)(3)} {Ni(2,2'-bpy)(2)(H2O)} {(Mo5O15)(4,4'-dbp)} (.) (4.75H(2)O)] (3), have been synthesized under hydrothermal conditions. Their structures were determined by single crystal X-ray diffraction. The 1-D chains is constructed of [Mo5O15(4,4'-dbp)](4-) units, which are further decorated and charge compensated by [M(1,10-phen)(2)] (M = Ni, Co) or [Ni(2,2'-bpy)(2)] subunits. The thermogravimetric analyses and magnetic properties of 1 and 2 were studied. (c) 2005 Elsevier Inc. All rights reserved.
引用
收藏
页码：1349 / 1355
页数：7
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