Collecting and processing neutron fibre diffraction data from a single-crystal diffractometer

被引:20
|
作者
Langan, P
Denny, RC
Mahendrasingam, A
Mason, SA
Jaber, A
机构
[1] UNIV LONDON IMPERIAL COLL SCI TECHNOL & MED,BLACKETT LAB,BIOPHYS SECT,LONDON SW7 2BZ,ENGLAND
[2] UNIV KEELE,DEPT PHYS,KEELE ST5 5BG,STAFFS,ENGLAND
关键词
D O I
10.1107/S0021889896002816
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The geometries for scanning reciprocal space for a fibre on a neutron single-crystal diffractometer are considered. Geometrical relationships are derived for the particular case of D19 at the Institut Laue-Langevin that can be readily generalized for other instruments and for the same instrument with a different detection system. An optimum data-collection strategy is proposed. Methods for processing neutron fibre data collected using this strategy are described and illustrated by studies on cellulose.
引用
收藏
页码:383 / 389
页数:7
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